Hi Marco

Further to Pedro’s comment, one way to avoid missing data in cusps is to use a 
multi-sweep strategy for data collection (as championed by the good folk at 
Global Phasing over many years). Many of the problems encountered in structure 
solution can be traced back to a sub-optimal data collection.

You don’t say which beamline at ALS you used, but if it’s got a kappa or 
similar fitted the beamline staff should be able to help.

best wishes

Harry

> On 20 Feb 2024, at 09:20, Pedro Matias <mat...@itqb.unl.pt> wrote:
> 
> Hi Marco,
> 
> Further to Zhen's comment, that can also happen if you have a cusp containing 
> one of the reciprocal lattice axes. The SG may be P212121 but one of the 21 
> is never located due to the missing data.

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