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Hi Jaishin,

You have to rename the CD atoms of your ILE residues to CD1. For some
reason CNS likes to call these atoms CD, while refmac calls them CD1.
You have a lot of them, so refmac produces a long list of warnings,
which compel it to stop.

Cheers,


Miguel

劉家欣(OZ) wrote:
> Dear All:
>    A dataset was indexed as R3 space group and subjected into CNS 1.1
> program as molecular replacement.
> Fortunately, a specific solution was obtained with high c.c value. With
> inspection of the pdb and density map, most part were fitted.
> However, the pdb doesn't refine by refmac 5.0 module of CCP4 5.0.2 version.
> A fatal error was showed and program was halted.
> I have no idea about that.
> Any helps would be high appreciated.
> Thank you very much.
>  
>  
>  
> jaishin
>  
>  
>  
>  --- title of input coord file ---
>  
>   PDB_code:XXXX
>   PDB_name:----
>   PDB_date:XX-XXX-XX
>   --------------------------------
>   WARNING : atom :CD   ILE      AA   7  is absent in the library
>   ATTENTION: atom:CD1  ILE      AA   7  is missing in the structure
>   WARNING : atom :CD   ILE      AA   9  is absent in the library
>   ATTENTION: atom:CD1  ILE      AA   9  is missing in the structure
>   WARNING : atom :CD   ILE      AA  15  is absent in the library
>   ATTENTION: atom:CD1  ILE      AA  15  is missing in the structure
>   WARNING : atom :CD   ILE      AA  16  is absent in the library
>   ATTENTION: atom:CD1  ILE      AA  16  is missing in the structure
>   WARNING : atom :CD   ILE      AA  31  is absent in the library
>   ATTENTION: atom:CD1  ILE      AA  31  is missing in the structure
>   WARNING : atom :CD   ILE      AA  47  is absent in the library
>   ATTENTION: atom:CD1  ILE      AA  47  is missing in the structure
>   WARNING : atom :CD   ILE      AA  50  is absent in the library
>   ATTENTION: atom:CD1  ILE      AA  50  is missing in the structure
>   WARNING : atom :CD   ILE      AA  66  is absent in the library
>   ATTENTION: atom:CD1  ILE      AA  66  is missing in the structure
>   WARNING : atom :CD   ILE      AA  74  is absent in the library
>   ATTENTION: atom:CD1  ILE      AA  74  is missing in the structure
>   WARNING : atom :CD   ILE      AA  92  is absent in the library
>   ATTENTION: atom:CD1  ILE      AA  92  is missing in the structure
>   WARNING : atom :CD   ILE      AA 110  is absent in the library
>   ATTENTION: atom:CD1  ILE      AA 110  is missing in the structure
>   WARNING : atom :CD   ILE      AA 117  is absent in the library
>   ATTENTION: atom:CD1  ILE      AA 117  is missing in the structure
>   WARNING : atom :CD   ILE      AA 149  is absent in the library
>   ATTENTION: atom:CD1  ILE      AA 149  is missing in the structure
>   WARNING : atom :CD   ILE      AA 155  is absent in the library
>   ATTENTION: atom:CD1  ILE      AA 155  is missing in the structure
>   WARNING : atom :CD   ILE      AA 164  is absent in the library
>   ATTENTION: atom:CD1  ILE      AA 164  is missing in the structure
>   WARNING : atom :CD   ILE      AA 167  is absent in the library
>   ATTENTION: atom:CD1  ILE      AA 167  is missing in the structure
>   WARNING : atom :CD   ILE      AA 173  is absent in the library
>   ATTENTION: atom:CD1  ILE      AA 173  is missing in the structure
>   WARNING : atom :CD   ILE      AA 175  is absent in the library
>   ATTENTION: atom:CD1  ILE      AA 175  is missing in the structure
>   WARNING : atom :CD   ILE      AA 189  is absent in the library
>   ATTENTION: atom:CD1  ILE      AA 189  is missing in the structure
>   WARNING : atom :CD   ILE      AA 196  is absent in the library
>    ... and more ...
>   ATTENTION: atom:CD1  ILE      AA 196  is missing in the structure
>    ... and more ...
>  
>  Spacegroup information obtained from library file:
>  Logical Name: SYMINFO   Filename: C:\CCP4win5.0.2\lib\data\syminfo.lib
>  
>  End of this subr
>   Number of chains                  :       2
>   Total number of monomers          :     696
>   Number of atoms                   :    5402
>   Number of missing atoms           :      66
>   Number of rebuilt atoms           :       0
>   Number of unknown atoms           :      66
>   Number of deleted atoms           :       0
>  
>   Number of bonds restraints    :    5360
>   Number of angles restraints   :    7282
>   Number of torsions restraints :    3606
>   Number of chiralities         :     870
>   Number of planar groups       :     928
>  IERR =            1
>  
> There is error. See above
> ===> Error: Fatal error. Cannot continue
> <B><FONT COLOR="#FF0000"><!--SUMMARY_BEGIN-->
>  Refmac_5.2.0005:  Fatal error. Cannot continue
> Times: User:       0.0s System:    0.0s Elapsed:     0:17 
> </pre>
> </html>
> <!--SUMMARY_END-->

- --
Miguel Ortiz Lombardía
Centro de Investigaciones Oncológicas
C/ Melchor Fernández Almagro, 3
28029 Madrid, Spain
Tel. +34 912 246 900
Fax. +34 912 246 976
email: [EMAIL PROTECTED]
www: http://www.ysbl.york.ac.uk/~mol/
~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
Je suis de la mauvaise herbe,
Braves gens, braves gens,
Je pousse en liberté
Dans les jardins mal fréquentés!
                                                       Georges Brassens
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