Dear all,
I have 8 data set from insulin at 1.2 A, after used Mosflm and Scala I
used tha program Sortmtz to reset the batch number, first, and after
unsorted MTZ files in one mtz file.
When I put this mtz file in SCALA I have the follow error message:
**** Insufficient data to determine parameters ****
0 reflections, 138 parameters
Scala: *** Too few reflections ***
Times: User: 30.2s System: 0.6s Elapsed: 0:31
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* Information from CCP4Interface script
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The program run with command: scala HKLIN
"/home/rgiordan/sortInsulin/prova7.mtz" HKLOUT
"/home/rgiordan/sortInsulin/sortInsulin_38_1_mtz.tmp" SCALES
"/home/rgiordan/sortInsulin/sortInsulin_38.scala" ROGUES
"/home/rgiordan/sortInsulin/sortInsulin_38_rogues.log" NORMPLOT
"/home/rgiordan/sortInsulin/sortInsulin_38_normplot.xmgr" ANOMPLOT
"/home/rgiordan/sortInsulin/sortInsulin_38_anomplot.xmgr" PLOT
"/home/rgiordan/sortInsulin/sortInsulin_38_surface_plot.plt" CORRELPLOT
"/home/rgiordan/sortInsulin/sortInsulin_38_correlplot.xmgr"
has failed with error message
Scala: *** Too few reflections ***
***************************************************************************
#CCP4I TERMINATION STATUS 0 " Scala: *** Too few reflections ***"
#CCP4I TERMINATION TIME 14 May 2009 14:59:13
#CCP4I MESSAGE Task failed
I tried to merge only the first 5 mtz files and SCALA works properly,
after I processed the latest 3 and everything is ok, but when I use the
8 files together i have problem.
Somebody know why I have this kind of problem?
Thank in advance.
Best regards,
Rita Giordano
