Hi all, Thank you all how have replied for their kind suggestions and diagnosis of collected data.
sincerely Debajyoti On Sat, 26 Mar 2011 04:44:42 +0530 wrote > > Hi all, > > I have collected one iodine soaked data in our home source, and processing the data using HKL2000. Exposure time per frame is 5min/1 degree. > While processing I have noticed that the Chisq values, cell parameters and rotation change Vs frame are deviating like anything. Please find the picasa link to see the carves. I will be benefited if anyone kindly suggest me the possible cause of these deviations. > > https://picasaweb.google.com/118341875228875389610/Mar252011?authkey=Gv1sRgCJXe6-ncmt6KmwE# > > Thank you all for your suggestions, > > Sincerely, > > Debajyoti