Dear Navin, As others have pointed out, it is not clear where your problem exactly lies: Are you not able to process the 2theta=20° run, or are you not able to merge it with the 2theta=0° run? Anyways, I and others have had similar problems with merging high and low resolution runs, see a very recent thread below:
http://www.mail-archive.com/ccp4bb@jiscmail.ac.uk/msg30764.html In my case, Scala would fail with low redundancy data or when there are too few reflections in common between both runs. What worked for me is to process with XDS and scale with XSCALE. For this you can use the autoProc procedure of global phasing, or teh Xia2 pipeline which seems to be part of CCP4. Using one of these pipelines will probably also solve your problem if you are not able to process the swing-out run. Good luck! Herman ________________________________ From: CCP4 bulletin board [mailto:CCP4BB@JISCMAIL.AC.UK] On Behalf Of navin narayanan Sent: Tuesday, April 09, 2013 1:49 PM To: CCP4BB@JISCMAIL.AC.UK Subject: [ccp4bb] 2Theta data set solving problem Hello everybody, We have a diffraction data set from home source with 2theta at 20deg. But we are not able to solve the data set using CCP4 suite. The software is picking up only the lower resolution data but not the higher resolution data points. Also we are not able to merge data two sets, one with 2theta at 0deg and the other with 2theta at 20deg. Is there anyway to solve the data. Any help will be truly appreciated. Thank you in advance. Navin V Narayanan
