Hi Tim

One last option that's possibly even better, but requires rudimentary
electronics: if you find the logic gate that flips from 0 to 1 (or
backwards) upon thermocouple triggering below threshold temperature, you
can simply supply +5V to the appropriate spot on the PCB, and Bob's your
uncle.

To find the spot one has to trace the connection a bit, and have a handy
voltmeter with a circuit probe, so when you put the TC into cold, it will
register the signal. This assumes a fairly simple operation of the
circuit - it may be that something much more sophisticated is taking place,
like a signal on a CAN bus or god knows what else.

All the best,

Artem
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On Fri, Feb 3, 2023 at 2:16 AM Tim Gruene <tim.gru...@univie.ac.at> wrote:

> Hi Artem,
>
> the simulator is exactly what I was looking for - many thanks!
> We did build a small circuit to generate the voltage (-0.586mV for
> -15C), but this didn't work - probably, our circuit was too simple. 12V
> input looks energetically better to me than using a peltier chiller (I
> meant peliter, not piezo originally...)
>
> Second to that I like Mark's idea of a long cable for the couple and
> stick it in the next -20C cooler.
>
> And yes - I already confirmed with cooling by liquid nitrogen, that the
> concept works: when the thermocouple indicates cold enough, I can
> operate the diffractometer, and hence install our new alien detector. I
> was indeed looking for a long-term solution to make overnight
> measurements.
>
> Thanks to everyone. I feel overwhelmed with the large number of quick
> responses.
>
> Best,
> Tim
>
> On Thu, 2 Feb 2023 20:19:32 -0500
> Artem Evdokimov <artem.evdoki...@gmail.com> wrote:
>
> > A basic Peltier element will likely work (may need a stack of two to
> > reach -20) however the simpler option indeed would be to 'fake out'
> > thermocouple input using a voltage, as described by Ivan.
> >
> > https://us.flukecal.com/Thermocouple-Temperature-Calculator
> >
> > And for $38 one can apparently purchase a thermocouple simulator
> >
> >
> https://www.brightwinelectronics.com/product/temperature-calibrator-k-n-thermocouple-generator-simulator
> >
> > Artem
> >
> > On Thu, Feb 2, 2023, 3:42 PM Rajkovic, Ivan <
> > 000095c2dc0d4fa4-dmarc-requ...@jiscmail.ac.uk> wrote:
> >
> > > Hi Tim,
> > >
> > > Not sure if this would work, but can you get a voltage supply and
> > > connect it instead of the thermocouple? You would need something to
> > > provide a few mV:
> > > https://www.thermocoupleinfo.com/type-k-thermocouple.htm
> > >
> > >
> > > Ivan
> > >
> > >
> > > > -----Original Message-----
> > > > From: CCP4 bulletin board <CCP4BB@JISCMAIL.AC.UK> On Behalf Of Tim
> > > > Gruene
> > > > Sent: Thursday, February 02, 2023 11:57 AM
> > > > To: CCP4BB@JISCMAIL.AC.UK
> > > > Subject: [ccp4bb] small scale -15C chiller
> > > >
> > > > Good day,
> > > >
> > > > I would like to cool a K-type thermocouple down to -15C. The
> > > > temperature
> > > does
> > > > not need to be very accurate, nor exactly -15C, just below that
> > > > level.
> > > >
> > > > I was thinking of using a piezo-chiller, but they don't seem to
> > > > be very
> > > energy
> > > > efficient.
> > > >
> > > > Could anyone make a recommendation for a simple device to cool
> > > > the tiny thermocouple to -15C to -20C?
> > > >
> > > > For the details: we have an inhouse diffractometer with a dead
> > > > detector.
> > > The
> > > > system is blocked, because the temperature of the detector needs
> > > > to be
> > > below -
> > > > 15C. It is measured with a K-type thermocouple. I tested with
> > > > liquid
> > > nitrogen.
> > > > The system show -64C (probably the limit of the thermocoupe) and
> > > > I can
> > > operate
> > > > the system (and mount our new (brand-alien) detector).
> > > >
> > > > Thanks a lot!
> > > >
> > > > Best,
> > > > Tim
> > > >
> > > > --
> > > > --
> > > > Tim Gruene
> > > > Head of the Centre for X-ray Structure Analysis Faculty of
> > > > Chemistry
> > > University
> > > > of Vienna
> > > >
> > > > Phone: +43-1-4277-70202
> > > >
> > > > GPG Key ID = A46BEE1A
> > > >
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>
> --
> --
> Tim Gruene
> Head of the Centre for X-ray Structure Analysis
> Faculty of Chemistry
> University of Vienna
>
> Phone: +43-1-4277-70202
>
> GPG Key ID = A46BEE1A
>

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