Looks like classic, poorly-diffracting “potato” crystals to me.
Will need additional optimisation to convince them into a nicer morphology.
No diffraction indicates that they are likely not to be salt at least.

Tony.


Antony W Oliver FHEA, PhD
Principal Research Fellow
Genome Damage and Stability Centre
Science Park Road
University of Sussex
Falmer, Brighton, BN1 9RQ





(office): +44 (0)1273 678349
(lab): +44 (0)1273 677512

antony.oli...@sussex.ac.uk<mailto:antony.oli...@sussex.ac.uk>; (he/him)
https://tinyurl.com/aw-oliver
https://orcid.org/0000-0002-2912-8273

________________________________
From: CCP4 bulletin board <CCP4BB@JISCMAIL.AC.UK> on behalf of 
careinaedgo...@yahoo.com <000002531c126adf-dmarc-requ...@jiscmail.ac.uk>
Sent: 08 November 2023 15:00
To: ccp4bb <ccp4bb@jiscmail.ac.uk>
Subject: [ccp4bb] What could these crystals be?

Hi all
We have been trying with no success to crystalize a protein. Recently we got 
these strange shape "crystals". They are hard and flat but they do not diffract 
at all. Any ideas as to what could cause this?
Careina

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