In Instance 32:7 Valerie Tomlinson asks for information about a black inlay 
material containing tin.

The inlay may original have been tin, which has now oxidised to a dark grey or 
black hydrous oxide, SnO2.Nh2O - this would explain your XRF signal.  
Unfortunately these hydrous oxides are often poorly crystallised so do not give 
a good X-ray diffraction pattern; however, it may be possible to identify it by 
its infra-red spectrum.

Barry Knight
St Albans
England

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