Here are reference spectra. The calibration is defined with the Fe metal edge
at 7110.75eV. The maghemite spectrum has been corrected for mild
overabsorption by reference to magnetite, which is very similar. The magnetite
is synthetic Fe3O4 from Aldrich, and done in TEY, so no overabsorption.
The maghemite is from oxidation of Fe oxide nanoparticles and has been verified
by XRD and comparison with the ETH group's maghemite spectrum.
mam
On 8/13/2013 1:33 AM, Teck Kwang Choo wrote:
Hi all,
@Drew Latta: I was wondering why the end members should be magnetite and
maghemite. Is it because they are both of inverse-spinel structure, the
difference only being that the latter has all Fe completely oxidized into
Fe(III)? Would you be able to provide the standard spectra to me if that is the
case? Thanks very much!
Previously I have only thought of using hematite (alpha-Fe2O3) and FeO as
end-members, both representing Fe(III) and Fe(II) respectively without giving
much thought to the structure Fe takes. I also had my doubts using magnetite
(Fe3O4) as a standard as it is a mixture of both Fe (II) and Fe (III). But
thanks to the insights Drew has given, I now think I should take the
Fe-coordination environment into account with the use of magnetite and
maghemite as standards.
@Alexandre and Matthew: I have obtained Mossbauer spectra of some of my samples
but like Drew said, it is not straightforward at this point in time. Will see
what I can do with the data I have!
Thanks for all your responses! It is greatly appreciated! This forum has been
more helpful than I thought!
Teck Kwang
On 13 August 2013 01:34, Matthew Marcus <mamar...@lbl.gov
<mailto:mamar...@lbl.gov>> wrote:
While it's true that Mossbauer is the gold standard for Fe valence
determination, access to the technique isn't all that common, and I don't know
of any facility that can do it on a micro scale. Is there one?
mam
On 8/12/2013 7:01 AM, Alexandre dos Santos Anastacio wrote:
Hello,
maybe that fingerprinting technique would be Mossbauer spectroscopy.
The Fe(II)/Fe(III) ratio comes easily and also there are lots of papers about
Mg-ferrite, an example:
10.1109/TMAG.2009.2018880 <http://dx.doi.org/10.1109/__TMAG.2009.2018880
<http://dx.doi.org/10.1109/TMAG.2009.2018880>>
Alexandre.
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Monash University
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#%Name: Maghemite nano powder
#%Empirical formula: gamma-Fe3+2O3 /Webmineral
#%Mineral group: oxides
#%Xtal system: cubic
#%Edge: K
#%Sample prep: powder on Kapton tape
#%Beamline: ALS 10.3.2, HxV slits = 200x20 um
#%Det: I0=N2, Fluorescence mode (Ge solid state 7elts)
#%Ref/notes: Mineralogical Research Company, San Jose, CA-USA. XRD confirmed.
#%Temp: Room temp (28C)
#%Time&date: 6:20 AM 7/3/2007
#%Provider: Matthew A. Marcus, Sirine Fakra.
#%============================================================
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