I do it just fine with Si111 (ALS 10.3.2).  Do you have some evidence that the 
energy resolution or flux isn't what it should be?  For instance,
have you recorded a S XANES spectrum on sulfate?  That has a sharp, intense 
peak.
        mam

On 5/11/2015 8:16 AM, Lisa Bovenkamp wrote:
Hello.
After having some troubles recording a good EXAFS spectrum with some old 
InSb111 crystals
I started wondering if it might be better to use Ge220 instead.
Anybody have some experience with that?

Lisa

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