http://www.sciencedaily.com/releases/2006/08/060807121419.htm
 

Source:  <http://www.aoac.org> AOAC International
Posted: August 7, 2006
 

Standard Developed For Collection Of Suspicious Powders

Federal, state, and local agencies have reached consensus on the first
validated national standard for collecting, packaging, and transporting
samples of visible powders that are suspected of being biological threat
agents, such as anthrax. The new standard meets the needs of the first
responders to test the powders on site, and the needs of the federal
agencies to conduct tests on the same, uncontaminated powder samples for
forensic and confirmatory analysis.
 
The national sample collection procedure was developed and approved by AOAC
INTERNATIONAL, which is a worldwide provider and facilitator in the
development of analytical standards. The new standard is applicable to
nonporous surfaces only and incorporates reference guidance for packaging
and transport of suspicious powders to comply with all appropriate federal
regulations regarding bio-safety and bio-security. 
The development and testing of the standard were supported by the Science &
Technology Directorate of the Department of Homeland Security (DHS) in
response to a need for a coordinated effort with federal agencies and
emergency responders to standardize activities related to anthrax and other
biological agent incidents.
"The development of this AOAC/ASTM standard represents an important step
towards building consensus between the emergency responder communities and
the federal agencies on national standards for responding to possible
terrorist attacks," said Bert M. Coursey, Director of DHS Office of
Standards. [For reference to ASTM, see last page of release.]
The purpose of the sampling procedure is to have a standard that is accepted
and followed by emergency responders for suspicious powder collection in
order to reduce exposure risks, reduce the variability associated with
sample handling and analysis, and increase the reliability of sampling
visible powders from nonporous surfaces. 
Emergency responders need to sample a suspicious powder in order to do a
presumptive analysis. Federal agencies also need a sufficient quantity of
the powder to do confirmatory testing. The new method provides both groups
with sufficient powder to perform their tests in a manner that protects the
powder from contamination. Training emergency responders who collect and
disseminate the powder is planned.
"The development of a national standard for the collection of suspicious
powders is an important step forward," said Chief John Eversole (Ret),
Chairman, Hazardous Materials Committee, International Association of Fire
Chiefs. "This standard provides a uniform and systematic procedure whereby
accurate, presumptive information can be determined by the First Responders
and ensure the preservation of sample evidence for confirmatory analysis and
criminal prosecution. Our next step must be to broaden the scope to do
sampling in other situations." 
"This is a major achievement. With this standard, a confidence can exist
among all of the partners engaged in the response, testing and investigation
of suspected biological agent releases," said David Ladd, Director,
Hazardous Materials Emergency Response for the Commonwealth of
Massachusetts, Department of Fire Services.
The sample collection standard is a two-step procedure that is performed
after an initial risk assessment is conducted and a visible powder is deemed
a credible biological threat. 
The first step of the procedure, or Method A, covers the bulk collection and
packaging of the suspicious visible powders from solid nonporous surfaces.
Bulk samples are collected and transported in a manner that permits public
health and safety, and law enforcement agencies to obtain uncompromised
samples for confirmatory analysis and forensic testing. The second step, or
Method B, covers swab sampling of residual suspicious powders for
presumptive on-site biological screening. 
A study was conducted in March 2006 to validate the reliability of the
sampling procedure at the U.S. Army Dugway Proving Ground. The study
demonstrated that the sampling procedure can be used by trained emergency
responders in simulated emergency conditions to consistently recover
samples. The study also proved that sufficient number of Bacillus anthracis
spores can be detected by emergency responders to make a presumptive,
on-site determination even after all bulk samples have been collected. The
evaluation study was designed to determine the recovery efficacy on seven
environmental surface types that included stainless steel, food-grade
painted wood, rubber, tile, concrete, finished wood, and plastic. 
The study involved six teams, including four National Guard Civil Support
Teams, the Navy's Chemical Biological Incidence Response Force (CBIRF) as
well as a hazmat team from the Florida Hazard Materials Response Unit. Team
members were dressed in Class C personal protective equipment during the
entire study so that the efficacy of the sample collection procedure could
be tested under as close to real-life conditions as could be attained.
The development of the sample collection standard was a cooperative,
interagency effort involving many stakeholder organizations including
federal, state, and local governments. Member organizations serving on the
AOAC Sampling Standard Task Group included the federal agencies NIST, CDC,
FBI, DOD, EPA, the U.S. Army Dugway Proving Ground, and the DHS Center for
Domestic Preparedness (CDP). State and local organizations represented
included the New York State Department of Health, State of Florida,
International Association of Fire Chiefs, and the U.S. National Guard.
Volunteers from ASTM Committee E54 and the AOAC Official Methods Board also
provided extensive review and input. 
The standard developed by AOAC has been published by ASTM INTERNATIONAL
under the title Standard Practices for Bulk Sample Collection and Swab
Sample Collection of Visible Powders Suspected of Being Biological Agents
from Nonporous Surfaces, E2458. It is available by contacting ASTM
INTERNATIONAL, 100 Barr Harbor Drive, PO Box C700 West Conshohocken, PA
19428-2959, www.astm.org <http://www.eurekalert.org> .
 
 


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