Markus If you don´t want to loose your data points, you can edit the "fullprof.dim" file to define the dimension of the arrays in fullprof. The first value MAXPOINT value defines the maximum number of data points in your experimental data.
A copy of this file should be in the same directory of your pcr file Regards Carlos Andre On Fri, 22 Jan 2010 12:07:59 +0100, amartin wrote > Hi Markus, > > youre right. When I put Ste=2 the program runs, even if half experimental > points are lost. It seems that with this FP version the step size of > the diffraction pattern must be larger. > > Thank you, > Alberto > > Scrive Markus Valkeapää <markus.valkea...@tkk.fi>: > > > Hi! > > Just a thought but increasing parameter "Ste" might help. From FullProf > > manual: > > -- > > ISTEP=1,2,3,.. If ISTEP>1 the number of data points is reduced by > > (Ste) a factor of ISTEP. Only those points corresponding to the > > new step size ISTEP*STEP (see Line #3 below) are taken > > into account in the refinement. Useful for speed-up > > preliminary refinements. > > -- > > In EdPcr Refinement/Reduction factor of number ... > > > > Best Regards, > > Markus Carlos André de Castro Pérez Físico Pesquisador - Núcleo de Catálise Programa de Engenharia Química - COPPE research in Chemical Engineering. +++++++++++++++++++++++++++++++++++++++++++++++++++++
