Re: [meteorite-list] Nickel found in hematite and magnetite?

2011-03-15 Thread Jim Wooddell
On Sun, Mar 13, 2011 at 7:26 PM,  cdtuc...@cox.net wrote:
 Dan.
  thank you for your info but,
 There is no way we are talking about the same XRF gun.
 Blain's gun does in fact give data in percentages as if the rock was assayed.
 I saw it with my own eyes. We did several test samples of real and well known 
 meteorites. During this test we read the digital results directly from the 
 gun itself and then compared the knows with the percentage results from the 
 gun.

Hello Carl and all!

I had the opportunity of watching this gun in action and let me tell
you, what a great compliment to the Tucson show it provided.  There
were some interesting rocks at the show that would have been
leaverites for a lot longer period of time without that gun.
While it's a major investment, I do hope that the thing pays for
itself over time.  It can do so much, there is opportunity to use it
well beyond meteorites.
With the gun being there at the show, it relieved a lot of tension
knowing we could run over there and shoot a stone!  Awesome!  It was
greatly appreciated.
One question I had about the gun, although I think this would be the
norm...can the file it creates be parsed and sent in a human readable
format?  IOW's, shoot a rock and later download the file and send the
results to the rock owner??

BTW, I think a demo of this unit and a small talk about it would make
for a good Pre-Blood Auction program prior to the auction.

Cheers!

Jim Wooddell
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Re: [meteorite-list] Nickel found in hematite and magnetite?

2011-03-13 Thread cdtucson
Paul,
I find tons of what you are describing.
Color tests work on almost any amount of nickel and also give false positives 
based on knowing exactly what shade of red to look for. I don't know which red 
is the correct red.
I have an AXE that tests bright red with a red color nickel test but in 
actually only has only a trace amount of nickel and scientists believe it needs 
more than just a trace. I may never understand why that is. I have been told 
that  nature has no way of separating the metals  but if that is true then 
why is there always a different percentage of nickel and why can it be as high 
as 60-ish percent and as low as just a few percent? 
That said,  If it is a highly  oxidized iron meteorite it would have a 
relatively high percentage of nickel as opposed to just a trace percentage. 
Blain's XRF gun gives complete analysis in percentages and would tell you if it 
has several percent nickel. if it does then the core of the rock may still be 
shiny iron. You could cut it in half and look inside. 
Blain offers this service and it is quick and inexpensive. Well worth the cost 
and the only way to be certain. 
Carl
--
Carl or Debbie Esparza
Meteoritemax


 Paul  G. Spears pgspe...@cox.net wrote: 
 In a specimen that may be a hematite, a strong presence of nickel was found. 
 Is that possible?  While the specimen is very attractive to magnets, tests 
 positive for nickel, and looks and weighs like iron, it has many pock marks 
 and some white inclusions that may be quartz.  Anyone come across similar 
 specimens? 
 
 
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Re: [meteorite-list] Nickel found in hematite and magnetite?

2011-03-13 Thread Dan Wray

Carl,

You are right, the nickel chemical test has lots of problems with false 
positives, not to mention a short shelf life after mixing.  On the subject 
of XRF guns, they will tell you that nickel is present but not the 
percentage.  The software claims that, but it is bogus.  I am an operator 
for our XRF gun  at the Geology Museum at the Colorado School of Mines.  We 
have done extensive testing of this machine and found that it has severe 
limitations.  Here are the results of a study done at the museum:
1. XRF can only identify  elements and can predict almost nothing about 
quantities.
2. Most of the time it can identify the presence or absence of elements, but 
not all of the time.  The software will identify elements that aren't there. 
You have to read the spectra to determine if the alpha and beta lines are 
indeed there.  Large amounts of lead or iron, (i.e.. meteorites), will block 
other readings.
3. Avoid quantities, one can't even say that there appears that there is 3x 
as much A as B.  The only way this works is with man made alloys and pure 
samples that the machine can be calibrated to.


The only good part is that I can test for nickel with a high degree of 
accuracy in about 30 seconds and tell the meteorwrong bringer that I used a 
scientific test to prove, what I probably already knew, that what he has is 
definitely not a meteorite.  It has also allowed us to correct specimens in 
the collection that are mis- identified.


Blain, you need to come over to the museum, we have much to share.

Dan Wray

- Original Message - 
From: cdtuc...@cox.net
To: Paul G. Spears pgspe...@cox.net; meteoritelist 
meteorite-list@meteoritecentral.com

Sent: Sunday, March 13, 2011 9:37 AM
Subject: Re: [meteorite-list] Nickel found in hematite and magnetite?



Paul,
I find tons of what you are describing.
Color tests work on almost any amount of nickel and also give false 
positives based on knowing exactly what shade of red to look for. I don't 
know which red is the correct red.
I have an AXE that tests bright red with a red color nickel test but in 
actually only has only a trace amount of nickel and scientists believe it 
needs more than just a trace. I may never understand why that is. I have 
been told that  nature has no way of separating the metals  but if that 
is true then why is there always a different percentage of nickel and why 
can it be as high as 60-ish percent and as low as just a few percent?
That said,  If it is a highly  oxidized iron meteorite it would have a 
relatively high percentage of nickel as opposed to just a trace 
percentage.
Blain's XRF gun gives complete analysis in percentages and would tell you 
if it has several percent nickel. if it does then the core of the rock may 
still be shiny iron. You could cut it in half and look inside.
Blain offers this service and it is quick and inexpensive. Well worth the 
cost and the only way to be certain.

Carl
--
Carl or Debbie Esparza
Meteoritemax


 Paul  G. Spears pgspe...@cox.net wrote:
In a specimen that may be a hematite, a strong presence of nickel was 
found.
Is that possible?  While the specimen is very attractive to magnets, 
tests
positive for nickel, and looks and weighs like iron, it has many pock 
marks

and some white inclusions that may be quartz.  Anyone come across similar
specimens?


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Re: [meteorite-list] Nickel found in hematite and magnetite?

2011-03-13 Thread cdtucson
Dan.
 thank you for your info but,
There is no way we are talking about the same XRF gun.
Blain's gun does in fact give data in percentages as if the rock was assayed.
I saw it with my own eyes. We did several test samples of real and well known 
meteorites. During this test we read the digital results directly from the gun 
itself and then compared the knows with the percentage results from the gun.
We also did irons and the nickel showed in percentages. One guy brought in a 
mill ball that had NO nickel but known irons showed exactly the known nickel 
percentages. ie 6% or 12% etc...
In our tests the only real limitation the gun had was the measurement of the 
lighter elements but only that it did not define and or separate them.
It gave them as a bulk percentage such as ( light elements) LE= 42%-ish.
For that reason It also failed to give Cr which is a real bummer because Cr is 
a very telling thing in planetary material. 
As the moon has way more than earth for example. May be in the order of 100 x . 
Yes, You and Blain do need to talk because apparently his $40,000. gun does do 
a lot more than the one you have.
To be fair. Blains gun has different settings. We used the same setting ( miner 
) on the real known meteorites as we used on all of my samples to give us a 
basis for comparison. Yes, adjustments did have to be made according to Randy 
Korotev but, once you do the conversion from element to oxide the numbers match 
up pretty well with the known percentages in the known meteorites that we 
tested.
I should note that Blain has no intention of classifying meteorites. This is 
simply a weed to rule strange rocks out. Not to prove they are meteorites. We 
did end up with a few really good prospects though and this without wasting any 
scientists valuable time. 
Here is a list of the samples we tested for use in comparisons.;
NWA 4857 MARS
NWA 6355 LUNAR
NWA 4734 LUNAR
NWA 480 MARS
Again, We zapped the above meteorites with Blain's gun and then compared the 
percentages with the known published percentages and they were a very close 
match once we converted the elements to oxides . Which is how they are 
published in the bulletin.
So, I hope you and Blain do get together. It is hard to believe these match by 
coincidence alone? 
For those of you who may not know Blain. Blain Reed Meteorites  is a major 
meteorite dealer. 
Thanks,
Carl


--
Carl or Debbie Esparza
Meteoritemax


 Dan Wray daniel_w...@comcast.net wrote: 
 Carl,
 
 You are right, the nickel chemical test has lots of problems with false 
 positives, not to mention a short shelf life after mixing.  On the subject 
 of XRF guns, they will tell you that nickel is present but not the 
 percentage.  The software claims that, but it is bogus.  I am an operator 
 for our XRF gun  at the Geology Museum at the Colorado School of Mines.  We 
 have done extensive testing of this machine and found that it has severe 
 limitations.  Here are the results of a study done at the museum:
 1. XRF can only identify  elements and can predict almost nothing about 
 quantities.
 2. Most of the time it can identify the presence or absence of elements, but 
 not all of the time.  The software will identify elements that aren't there. 
 You have to read the spectra to determine if the alpha and beta lines are 
 indeed there.  Large amounts of lead or iron, (i.e.. meteorites), will block 
 other readings.
 3. Avoid quantities, one can't even say that there appears that there is 3x 
 as much A as B.  The only way this works is with man made alloys and pure 
 samples that the machine can be calibrated to.
 
 The only good part is that I can test for nickel with a high degree of 
 accuracy in about 30 seconds and tell the meteorwrong bringer that I used a 
 scientific test to prove, what I probably already knew, that what he has is 
 definitely not a meteorite.  It has also allowed us to correct specimens in 
 the collection that are mis- identified.
 
 Blain, you need to come over to the museum, we have much to share.
 
 Dan Wray
 
 - Original Message - 
 From: cdtuc...@cox.net
 To: Paul G. Spears pgspe...@cox.net; meteoritelist 
 meteorite-list@meteoritecentral.com
 Sent: Sunday, March 13, 2011 9:37 AM
 Subject: Re: [meteorite-list] Nickel found in hematite and magnetite?
 
 
  Paul,
  I find tons of what you are describing.
  Color tests work on almost any amount of nickel and also give false 
  positives based on knowing exactly what shade of red to look for. I don't 
  know which red is the correct red.
  I have an AXE that tests bright red with a red color nickel test but in 
  actually only has only a trace amount of nickel and scientists believe it 
  needs more than just a trace. I may never understand why that is. I have 
  been told that  nature has no way of separating the metals  but if that 
  is true then why is there always a different percentage of nickel and why 
  can it be as high as 60-ish percent and as low as just a few percent

[meteorite-list] Nickel found in hematite and magnetite?

2011-03-12 Thread Paul G. Spears
In a specimen that may be a hematite, a strong presence of nickel was found. 
Is that possible?  While the specimen is very attractive to magnets, tests 
positive for nickel, and looks and weighs like iron, it has many pock marks 
and some white inclusions that may be quartz.  Anyone come across similar 
specimens? 



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