[biofuel] Looking for tests to indicate quality of Methanol

2003-02-28 Thread Mark Foltarz

Group,

  I am looking for methods of analysis to indicate the water content of
Methanol.

  I would like to do this  in the "field" as it were. I have found several
methods of detecting the occurence of Methyl Alcohol in Ethyl. So these tests
are aimed at the foddstuffs industry rather than the quality of Methanol as
being technical grade - the all desireable 98.5%.

  The only contaminants I will be looking for is Ethanol and Water. I don't
believe there will be any other organic contaminants

 Specific gravity 
   Methyl is 0.7924  Water is 1. Ethanol is 0.816

 Fractional distallation  
   Boiling Point of Methanol is 115 C Water is of course 100 C Ethanol is 78 C

  Any other ideas?

  Mark   

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Re: [biofuel] Looking for tests to indicate quality of Methanol

2003-03-01 Thread Keith Addison

>Group,
>
>  I am looking for methods of analysis to indicate the water content of
>Methanol.
>
>  I would like to do this  in the "field" as it were. I have found several
>methods of detecting the occurence of Methyl Alcohol in Ethyl. So these tests
>are aimed at the foddstuffs industry rather than the quality of Methanol as
>being technical grade - the all desireable 98.5%.
>
>  The only contaminants I will be looking for is Ethanol and Water. I don't
>believe there will be any other organic contaminants
>
> Specific gravity
>   Methyl is 0.7924  Water is 1. Ethanol is 0.816
>
> Fractional distallation
>   Boiling Point of Methanol is 115 C Water is of course 100 C Ethanol is 78 C
>
>  Any other ideas?
>
>  Mark

Hi Mark

Boiling point of methanol is about 65 deg C (149 deg F).

If you plan to use it for biodiesel, a few percent lower purity might 
not matter too much. If the impurity is water though, it might matter 
if you're using WVO with high FFA levels. Small amounts of ethanol 
shouldn't matter either.

Best

Keith


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Re: [biofuel] Looking for tests to indicate quality of Methanol

2003-03-01 Thread Ken Provost

Mark writes:


>I am looking for methods of analysis to indicate the water content of
>Methanol. I would like to do this  in the "field".

Do a Google search on "cobalt chloride test paper". You tear off a bit,
dip it in your sample. Blue means real dry (fine for biodiesel), pink
means wet. It's very crude -- slightly pink will also work fine for
methanol, but is way too much water for ethanol. My guess is it starts
turning pink around 1.5% water. I use it all the time-K

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