Re: [Biofuel] Glycerin soap making

2005-02-16 Thread [EMAIL PROTECTED]


can some glycerin be added to new oil to make a soap?
Farmer Paul
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Re: [Biofuel] Glycerin soap making

2005-02-16 Thread Appal Energy



Glycerol is an alcohol. Fats/oils are required to make soap.

Todd Swearingen

- Original Message - 
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Cc: [EMAIL PROTECTED]
Sent: Tuesday, February 15, 2005 7:39 PM
Subject: Re: [Biofuel] Glycerin soap making




can some glycerin be added to new oil to make a soap?
Farmer Paul
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Re: [Biofuel] Glycerin soap making

2005-02-16 Thread Andrew Cunningham

Paul,

Do you mean glycerin or the glycerin layer as there is a big difference?

Andy


On Tue, 15 Feb 2005 23:19:28 -0800 (PST), [EMAIL PROTECTED]
[EMAIL PROTECTED] wrote:
 
 can some glycerin be added to new oil to make a soap?
 Farmer Paul
 [EMAIL PROTECTED]
 
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Re: [Biofuel] Glycerin soap making

2005-02-16 Thread Andrew Cunningham

You should be able to use the left over lye in the glycerin layer to
make soap, but it may end up have way too much glycerin in it and end
up be drying for the skin.

Andy

On Wed, 16 Feb 2005 02:40:12 -0500, Appal Energy [EMAIL PROTECTED] wrote:
 Glycerin can be added to any soap. But it can't be used to make soap.
 
 Glycerol is an alcohol. Fats/oils are required to make soap.
 
 Todd Swearingen
 
 - Original Message -
 From: [EMAIL PROTECTED]
 To: [EMAIL PROTECTED]
 Cc: [EMAIL PROTECTED]
 Sent: Tuesday, February 15, 2005 7:39 PM
 Subject: Re: [Biofuel] Glycerin soap making
 
 
  can some glycerin be added to new oil to make a soap?
  Farmer Paul
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Re: [Biofuel] Glycerin soap making

2005-02-15 Thread Legal Eagle


the other night having a good look through it. Simple and efficient. maybe I 
could make some ethanol (vodka) for tinctures :-) or a fuel additive, 
hehe.

Luc
- Original Message - 
From: JD2005 [EMAIL PROTECTED]

To: [EMAIL PROTECTED]
Sent: Tuesday, February 15, 2005 5:22 PM
Subject: Re: [Biofuel] Glycerin soap making




- Original Message -
From: Legal Eagle

G'day JD;

Using a simple to make condenser. There is an example at the bottom of 
the

5

gallon processor at JtF
http://journeytoforever.org/biodiesel_processor5.html . I have just

finished

one of these and am hooking it up to a pressure cooker. This is yet
experimental, so don't run out and do it. The first use worked so so.


Is this the same as the absolute alcohol process?Alcohol from 
methanol.

Or is that something different again?


JD2005


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Re: [Biofuel] Glycerin soap making

2005-02-15 Thread JD2005


- Original Message -
From: Legal Eagle
 G'day JD;

 Using a simple to make condenser. There is an example at the bottom of the
5
 gallon processor at JtF
 http://journeytoforever.org/biodiesel_processor5.html . I have just
finished
 one of these and am hooking it up to a pressure cooker. This is yet
 experimental, so don't run out and do it. The first use worked so so.

Is this the same as the absolute alcohol process?Alcohol from methanol.
Or is that something different again?


JD2005


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Re: [Biofuel] Glycerin soap making

2005-02-14 Thread Andrew Cunningham

You don't lose anything as you leave it in there on purpose, it adds to the
combustability of the glycerine log.
Luc


-Or you could just recover the alcohol before burning.

Andy
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Re: [Biofuel] Glycerin soap making

2005-02-14 Thread Andrew Cunningham

If you have a sealed container with a vent line, source of hot water
(above 75C) and cold water - yes.  Run the hot water around the sealed
container or put the sealed container in bath of hot water.  This will
boil off the MeOH - add hot water as needed.  The vapors will travel
out the vent.  The vent line can be coiled and placed in a cold water
bath and the open end of the coil then leads into your MeOH recovery
vessel.  As the coil fills with MeOH it will push out the liquid MeOH
into the recovery vessel.  It would be good to keep that vessel cold
as well and have the outlet of the tubing go down to the bottom of
that tank so any left over vapors will bubble through cold MeOH and
condense (there shouldn't be any... but).

Goggle for batch distillation and find out what each X from a XXX jug means.

Andy


 
  -Or you could just recover the alcohol before burning.
 
  Andy
 
 By evaporation...Is there an easy, non-expensive way of doing this using
 standard eqipment that could be purchased anywhere in the world (i.e. the
 UK)?
 
 
 JD2005
 
 
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Re: [Biofuel] Glycerin soap making

2005-02-14 Thread Legal Eagle



- Original Message - 
From: JD2005 [EMAIL PROTECTED]

To: [EMAIL PROTECTED]
Sent: Monday, February 14, 2005 2:04 PM
Subject: Re: [Biofuel] Glycerin soap making

By evaporation...Is there an easy, non-expensive way of doing this using
standard eqipment that could be purchased anywhere in the world (i.e. the
UK)?


Using a simple to make condenser. There is an example at the bottom of the 5 
gallon processor at JtF 
http://journeytoforever.org/biodiesel_processor5.html . I have just finished 
one of these and am hooking it up to a pressure cooker. This is yet 
experimental, so don't run out and do it. The first use worked so so. It 
evaporated the methanol although the lid wasn't secure enough and I got 
leakage of methanol and around a heat source that is counter-indicated as 
the stuff is very volatile, so I am modifying the lid of the pressure cooker 
to be more hermetically sealed in order to send all the vapours into the 
condenser.
My condenser is almost identical to the one at JtF except that I used T 
fittings for the water inlet and drain. The in/out side of the T is 
threaded for standard 2 and so I used a fine thread bung cap with 3/4 
thread incorporated in the cap and plumbed a hose barb to it and then 
clamped the hose onto the barb.
Sealing the end caps was also a challenge. I tried epoxy, but it cracked and 
leaked, so I then remembered using a thing called Goop 
http://www.naturalhandyman.com/iip/infxtra/infgoo.shtm to fix a bit of trim 
that had come loose on the Benz, and this is cold weather and damp as well 
and it is still holding perfectly a year later, so I Goop-ed the copper 
tubing exiting the end caps with this stuff and it is holding up quite 
nicely, no leaks. I hope to have pics available soon.I have pics of the 
condenser but am waiting until I can get the unit working properly before 
posting about it all.

Luc



JD2005


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Re: [Biofuel] Glycerin soap making

2005-02-14 Thread JD2005


- Original Message -
From: Andrew Cunningham


 -Or you could just recover the alcohol before burning.

 Andy

By evaporation...Is there an easy, non-expensive way of doing this using
standard eqipment that could be purchased anywhere in the world (i.e. the
UK)?


JD2005


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Re: [Biofuel] Glycerin soap making

2005-02-13 Thread Andrew Cunningham

Tracy,

I am currently taking classes towards a Masters in Health Product
Regulation.  I have spent a lot of time with various FDA regulations
and the way I would interpret most is that it has to  more than 50%
of the final product.  Therefore you could take pure soap and mix 49%
dirt into it and sell it as soap.  Not many people would buy 49% dirt
soap, but it would meet the FDA's description of Soap.  I would have
to lookup the definition of cosmetics to be sure, but the main
differences between soaps, cosmetics and drugs are what you claim it
does.

You are correct about the soap reaction, by-product glycerin can be
added to soap but cannot be made into soap.

My only suggestion on how to determine the amount of lye to use would
be to do small trial batches or some form of titration.

Andy


On Sat, 12 Feb 2005 00:50:47 -0800 (PST), Jeremy  Tracy Longworth
[EMAIL PROTECTED] wrote:
 My name is Tracy, and I am Jeremy's wife.  I am also a soapmaker.  There are 
 a few things that concern me about making soap with the by-product of 
 biodiesel.
 
 First, imho, the wvo is not exactly the cleanest stuff to begin with and I 
 think there might be problems with the government in producing soap with it.  
 The FDA defines soap as a product in which most of the nonvolatile matter 
 consists of an alkali salt of fatty acids and whose detergent properties are 
 due to these alkali-fatty acid compounds.  If I read the regulations 
 correctly, if a soap is made mostly of anything else, it is then considered 
 a cosmetic and comes under certain regulations.  True soap is not regulated 
 by the FDA: cosmetics are.
 
 Secondly, soap cannot be made from primarily glycerin.  Glycerin is a 
 by-product of soapmaking and is left in handmade soaps or extracted from 
 commercially made soaps.  The soap is formed from the reaction of a caustic 
 soda and fatty acids.  If anyone is truly making soap from the by-product of 
 making biodiesel, then it would stand to reason that there are left-over oils 
 in the glycerin.
 
 Third, there is no way to know for certain what kinds of oils comprise WVO.  
 Many restaurants don't always use the same kind of oil.  That being the case, 
 I can't see how one could accurately figure the amount of lye needed in order 
 to achieve proper saponification.  Every oil requires a different amount of 
 lye in order for it to properly saponify.  If one were to use too much lye, 
 the resultant soap would be lye heavy and too harsh for anyone to use.
 
 I did also see written that the lye was to be added to warm water, I believe. 
  I, and the soapmakers I am in contact with, add their lye to cold water.  
 When the lye is added to water, the resulting solution can reach temperatures 
 near boiling at times.  If one was to start out with warm water, the solution 
 could volcano and create quite a mess, not to mention it could also cause 
 harm to anyone around at the time.
 
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Re: [Biofuel] Glycerin soap making

2005-02-13 Thread Legal Eagle



- Original Message - 
From: JD2005 [EMAIL PROTECTED]

To: [EMAIL PROTECTED]
Sent: Sunday, February 13, 2005 5:20 PM
Subject: Re: [Biofuel] Glycerin soap making



Thank you for this thread.   It is one of the best threads at the moment
because it is constructive.

When you make boifuel you are left with alot of glycerin we all know that.
What we don't know is what this glycerin can be utilised for.

Also if the glycerin is from a wvo reaction to make rem or ree whether it 
is

suitable for making soap or not.


Yes, maybe, and that is the experimenting part :-)
There is a lot of info at JtF about soap making too, have you snooped it ?
Also about seperating the FFA's from the glycerine.
http://journeytoforever.org/biodiesel_glycsep.html
http://journeytoforever.org/biodiesel_glycerin.html



JD2005


Presumeably lye water would be realy an ideal method of making soap from
glycerin.


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Re: [Biofuel] Glycerin soap making

2005-02-13 Thread JD2005

Thank you for this thread.   It is one of the best threads at the moment
because it is constructive.

When you make boifuel you are left with alot of glycerin we all know that.
What we don't know is what this glycerin can be utilised for.

Also if the glycerin is from a wvo reaction to make rem or ree whether it is
suitable for making soap or not.


JD2005


Presumeably lye water would be realy an ideal method of making soap from
glycerin.


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Re: [Biofuel] Glycerin soap making

2005-02-13 Thread JD2005

Ok Thanks,

The burning idea with the milk cartons looks really good to us here.   We're
burning wood and stuff on an old oxfordshire range here at the moment.I
wouldn't put one on untill we'd got a really hot fire though because of the
poison fumes it can cause.Also you stand stand to lose methanol or
ethanol that way unless you separate that out.   The FFA separation with
some kind of expensive acid I reject on the grounds of expense.   Unless, I
could (I havn't got any methanol or a license for ethenol yet.) find a
market for the pure glycerin.

JD2005
- Original Message -
From:Legal Eagle
 G'day JD;

 Yes, maybe, and that is the experimenting part :-)
 There is a lot of info at JtF about soap making too, have you snooped it ?
 Also about seperating the FFA's from the glycerine.
 http://journeytoforever.org/biodiesel_glycsep.html
 http://journeytoforever.org/biodiesel_glycerin.html

 
  JD2005
 
 
  Presumeably lye water would be realy an ideal method of making soap from
  glycerin.
 
 



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