Re: [ccp4bb] Negative CCanom

2015-07-16 Thread Keller, Jacob
>Jacob's case is twinning in P3(2)12 making the data appear as P6(2)22, so it >is indeed a rotation by 180°. Yes, this all fits together nicely. If I understand correctly, this would make my crystals a blend of mero- and pseudo-mero-hedral, so involving I's and F's, no? JPK

Re: [ccp4bb] Negative CCanom

2015-07-16 Thread Keller, Jacob
Here is the answer, I think, to why twinning leads to negative CCanom: In fact, in any case in which the anomalous signal changes as a function of exposure, CCanom can be negative. The usual case is radiation damage: Consider, to start, four independent measurements of one reflection, two I+ an

Re: [ccp4bb] Negative CCanom

2015-07-16 Thread Keller, Jacob
[Sorry, typography was off a bit in the last one] Here is the answer, I think, to why twinning leads to negative CCanom: In fact, in any case in which the anomalous signal changes as a function of exposure, CCanom can be negative. The usual case is radiation damage: Consider, to start, four in