Re: [ccp4bb] missing layer of electron density

2007-03-01 Thread Eleanor Dodson
Such a "twinning operator" can also indicate that you spacegroup has an extra symmetry operator (h,-h-k,-l) That is in fact one of the symmetry operators for P3i21 H32 P6i22 Have you solved the structure in the lower symmetry and is that missing density properly generated by this operator?

[ccp4bb] missing layer of electron density

2007-02-27 Thread Benirschke, Robert C.
Dear all, I am trying to solve the structure of a protein complex, via MR, and when the phasing is complete there is 1/3 of the unit cell that is missing electron density. The density present looks very good and shows helices in regions that were disordered in my NMR model, suggesting that it