Re:Data collection strategy from low angles - Bruker D8 Advance, Lynx Eye XE detector

2016-10-21 Thread iangie
Dear Frantisek, >I have tried the 0.26 and 0.14° FDS, however a large "beam overflow" has >occurred. Moreover, the intensities of diffractions at higher angles are very >low in comparison to the data collected with ADS slits. [TW] At θ=1° , 0.26 and 0.14° FDS coresponding to ~39 and ~74 mm

SRM 1979 now available

2016-10-21 Thread Cline, James Dr. (Fed)
Hi all, The new NIST SRM for analysis of crystallite size that I have spoken about on a number of occasions over the years is now available. SRM 1979 - Powder Diffraction Line Profile Standard for Crystallite Size Analysis (Nano-Crystalline ZnO Powder)

Data collection strategy from low angles - Bruker D8 Advance, Lynx Eye XE detector

2016-10-21 Thread František Laufek
Dear all,   I would like to ask you about your experience in collecting the XRD data from low angles (for me from 2° of 2Theta) to 50° 2Theta using the Bruker D8 Advance diffractometer (Bragg-Brentano geometry) with the Lynx Eye XE position sensitive detector.     The studied samples are