Sounds like water...do you have any of the old WVO around? Try heating
it and see if if it spits - indicating water.
Is it glop or cloudy liquid?
Did you run a few test batches first?
-Mike
Golan Shmuel wrote:
> hay every one
> i was thinking that after 500 liter good quality b.d i left the b
Golan,
Just for grins and giggles, take a liter and boil out any residual
alcohol. Then see if anything settles out.
If not, dissolve one gram of catalyst in 40 ml of methanol and mix that
with 200 ml of your problem stock. Observe.
First guess is that your white layer was soap. A little unusu
hay every onei was thinking that after 500 liter good quality b.d i left the big mistakes behind me.any way the last batch i did yesterday turned out with no separation at all.it was 95 liter wvo titration
1.4. used 19 liter methanol & 466g laysame reactor and reaction time (90 min) as batches b
