> Just wondering if anyone bothers much about methanol extraction, and
> the whole issue about vacuum systems.
>
> Dave
..................

Yup. Some of us do. When running small batches, it may not seem to be of
much consequence, but it's about 5 gallons for every 50 gallons of output.
That's a boatload of toxic material to be flushing down the drain or washing
into a field.

Nothing like creating another dead zone on the farm.

Approximately 2% of the recoverable methanol is in the biodiesel. This
amounts to about half of one gallon in 300 gallon batches. The remaining 98%
recoverable is in the glycerin and amounts to ~29.5 gallons. At $1.50 or
more a gallon for methanol, you can see where recovery becomes cost
effective rather quickly.

The least energy intense method of recovery requires that the 120 degree
reaction temp is never lost - not even during a separation period. This
permits a rather quick jump up to evaporation temp for the alcohol, rather
than starting from scratch. The only way to achieve this is with a well
insulated system.

For shadetree operations, simple R-19 Kraft faced insulation secured to the
vessel(s) with 2" box tape does the trick. Larger reactors of several
hundred gallons or more would need spray insulation, which can usually be
acquired at any tank fabrication company.

Not only does the insulation reduce energy input during recovery, but during
the reaction as well.

After all, one of the purposes of making biodiesel is to reduce fossil fuel
consumption, yes?

Todd
Appal Energy
[EMAIL PROTECTED]



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