Since I signed on a few weeks ago, I have been researching like 
crazy the feasibility of small scale biodiesel from WVO in my 
community - rochester new york. 

my question is:  how to meet ASTM standards and the biggest 
problem I encounter is methanol RECLAIMATION.   So, if you have 
an answer, please forward.  if you are interested in my research so 
far, read on. 

a number of companies produce biodiesel to ASTM standards in 
the USA.  In particular, Ocean Air does a million gallons a month.  
They use the basic formula, tickell uses, NaOH, Methanol, WVO 
or Virgin (often Soy) oil. But, they reclaim methanol, purify 
glycerine to cosmetic grade, reclaim catalyst, purify out Fatty 
Acids AND have a patended capacity to produce fuel from 
reclaimed fatty acids.  Needless to say, they did not explain this to 
me.  However, if its patended, its available to enterprising research 
maniacs.  

Washing Biodiesel removes some fatty acids, all methanol from 
the biodiesel ( but not the glycerine unless you wash that too).  
Washing alone does not meet ASTM due to the residual fatty 
acids.   Biodisel.org either in a bow to soy growers or out of real 
concern for diesel engines prints for following text at 
http://www.biodiesel.org/perils_of_home-brew.htm

Their concern is free fatty acids, free methanol and engine wear.  
Washing alone leave fatty acids adn creates an environmental 
problem to anyone who want to make a quantity of product.

Another issue is density.  the Methanol content makes a true 
calculation of specific gravity impossible,  to really check that, you 
need a methanol free product.  To REALLY meet ASTM standards, 
http://www.biodiesel.org/default2.htm

one might need to do a gas chromotography analysis to check for 
unreacted components, acids etc.  

So, thats it for now...if anyone knows of a small scale production 
(over 100 gallons a week, under 1000 a week) and a inexpensive 
way to meet ASTM standards, follow up. 

Or, if you have evidence that some of these standards simply a 
mechanism to "corner the market" for agribusiness by creating a 
false notion WVO biodiesel is unmarketable, post it up. 

thanks .

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