Hello,
I have been trying to separate glycerin and FFA's with 210 ml phosphoric
acid in 1500 ml of the glycerin layer.
All that happens is, that the whole lot gets thicker and thicker, but no
separation at all.
What am I doing wrong ? The glycerin layer is not really liquid. I would say
about as thick as yoghurt.
I used 4 grams of lye in the BD proces ( in Holland the veg. oil has to be
refreshed every day, so I am lucky to gather allmost unused oil )

Met vriendelijke groeten,
Pieter Koole
Netherlands

----- Original Message -----
From: "appalenergy" <[EMAIL PROTECTED]>
To: <biofuel@yahoogroups.com>
Sent: Friday, June 20, 2003 1:23 AM
Subject: [biofuel] Re: Thanks for the answers Tod. Here are some more
questions.


> Peter,
>
> > > -Is there a way to do a proper titration on this job?
> > Why titrate? The feedstock is 100% FFAs.
> > * To detect how much acid I need to do a proper separation.
>
> Don't think you can separate 100% FFAs, at least not unless you want
> to fractionally distill them by carbon chain length.
>
> But I gather you mean "how much acid [you] need to do a proper
> [esterification]?"
>
> Durned good question. We've never tried esterification on 100% FFAs.
>
> Maria could probably tell you how high a FFA content she's seen
> processed at University of Idaho.
>
> > All oils are "harmfull" to some extent or another, smothering
> > whatever they cover. Just that veg oil is slightly less toxic than
> > fossil.
> > * I understand that, but my question is : Does it damage the
> roots, the leaves ? Telling people that I have a harmless
> weedkiller, sounds at least funny.
>
> Inhibits photosynthesis. Not systemic, such as Roundup and other
> chemical types.
>
> Todd Swearingen
>
>
>
>
>
>
> Biofuel at Journey to Forever:
> http://journeytoforever.org/biofuel.html
>
> Biofuels list archives:
> http://archive.nnytech.net/
>
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>


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