-
   Hello All,
 I asked some questions in my last post but didnt get any answers but 
Ill ask another one anyway and maybe someone will answer it.
Im assuming that when the unwashed biodiesel stratifies, that pretty 
much all the Glycerine-methanol and soap has settled beneath the 
biodiesel and that can be decanted.
 The washing process  to meet astm seems to take up a long time .. Is 
it feasable to distill the water-methanol mix out of the biodiesel 
rather than wait for it to separate and stratify?? or will trace 
elements of soap screw things up..?...any thoughts on this???
 Marc









-- In biofuel@yahoogroups.com, "Marc Orion Cardoso" <[EMAIL PROTECTED]> 
wrote:
> -
>   thanks for your good wishes, so far Ive had really good results  
> with  four consecutive litre batches of  new canola oil using the 
> usual 200 ml methanol and 3.5 grams of lye, agitating it for 
fifteen 
> minutes  with great results, a brandy coloured  layer of  glycerin 
> and a layer of soap with  the rest being fairly clear biodiesel, 
but 
> yesterday afternoon I used wesson brand soybean oil (new) and found 
a 
> clear layer at the bottom about 1/4 inch deep and the rest  of the 
> oil is cloudy it just doesnt seem to be a complete reaction. can 
you 
> tell me why the canola worked and the soy didnt seem to?
> MARC
> 
> 
> 
> 
> 
> 
> 
> 
> -- In biofuel@yahoogroups.com, Keith Addison <[EMAIL PROTECTED]> wrote:
> > Hello Marc
> > 
> > Glad you've passed the first hurdles with making biodiesel, good 
> for you.
> > 
> > Thanks for the information, and please do keep us informed of 
your 
> > progress, especially with extracting oil from the algae for 
> biodiesel.
> > 
> > Best wishes
> > 
> > Keith
> > 
> > 
> > 
> > >   Dear Kieth and lowell.
> > >
> > > We have been growing algae of various types for a good number of
> > >years starting with Spirulina as a food and then venturing into
> > >algaes suitable for lipid production.. First we had to learn to 
> grow
> > >algae and came to the level of designing a closed loop system 
that
> > >would allow the production of algaes under a broad range of 
> climatic
> > >and geographic  conditions ....in that, we succeeded... we have 
> been
> > >growing dunaliela and butyrococcus with success in our research 
> pond
> > >here at ecogenics center.. although we have been  producing 
ethanol
> > >and methane for many many years and were well aware of the 
> potential
> > >of algae for the production of lipids (oils) for biodiesel. we 
had
> > >not, untill very recently ,actually produced biodiesel.. we  
have 
> now
> > >reached that goal with a fair amount of consistancy and are now
> > >prepared to enter a  new phase in our development program... that
> > >is.. the extraction of oil from our algaes and the consequent
> > >production of biodiesel from the resulting oils. we are soon
> > >embarking on a program of study involving extraction techniques 
and
> > >after that will undertake the necessary steps to make biodiesel 
> from
> > >those oils.We are taking very cautious baby steps towards that
> > >goal.financial constraints have made it prudent to  go slowly and
> > >deliberatly in all our endeavours one look at our website and 
one 
> can
> > >see that we have touched  upon many areas of R&D over the 
years.we
> > >expect that with some wise investment of time and money we will
> > >successfully adress the extraction and production phase of the 
> algae
> > >to biodiesel program..we will of course keep you posted as to our
> > >progress....in the meantime we are ready to produce biodiesel 
from
> > >wvo...we have made the necessary modifications to our distillery 
so
> > >we can do this...
> > >    Marc...
> > >
> > >
> > >
> > >
> > >-- In biofuel@yahoogroups.com, Keith Addison <[EMAIL PROTECTED]> wrote:
> > > > Hi Lowell
> > > >
> > > > >A lot of lit on this subject during 1980s. Search on "NTIS" 
> which
> > >is U.S.
> > > > >gov repository for gov funded research. The critters you 
want 
> info
> > >on are
> > > > >called "Microalgae" not algae and they produce Lipids" which 
> you
> > >and I call
> > > > >"oil". If you want info about getting the oil out of the
> > >microalgae search
> > > > >on the net for "Lipid Extraction". Most of NTIS research on 
> this
> > >is under
> > > > >program called "Aquatic Species Program". Try to get 1987 
and 
> 1985
> > >reports.
> > > > >Each report cost me at least $30 to $60. Solar Energy 
> Institute in
> > >Golden
> > > > >CO. published a neat small report in 1985 called Fuel 
options 
> from
> > > > >Microalgae dated July 1984. If you get into this you will 
need 
> to
> > >buy quite
> > > > >a few chemicals, some common like Epsom Salt, baking soda 
and 
> some
> > >pretty
> > > > >exotic. If you want to look at "houses" for your critters 
> search
> > >on the net
> > > > >for "photobioreactor" . Tried this once and failed. Also 
wife 
> and
> > >daughters
> > > > >saw no humor in growing "pond scum" in the house. May try 
this 
> one
> > >day when
> > > > >I get some space out of the house but am more interested in
> > >finding cheap
> > > > >sources of oil seeds. Hope this helps. Good luck.
> > > >
> > > > You're not the first to reach that conclusion. Previously a 
list
> > > > member set up ponds and so on and was going ahead full-steam 
> but we
> > > > never heard any more about it. Another list member researched 
> the
> > > > subject, he had good technical resources, and concluded that 
> it's a
> > > > waste of time right now, it just isn't there yet, at least 
not 
> at a
> > > > doable small-scale level.
> > > >
> > > > Marc Carduso of Ecogenics has posted several upbeat messages 
on 
> the
> > > > subject in the last few weeks. He's talked of "Algae 
production 
> for
> > > > food fuel and fertiliser", "algaeculture technology for oil
> > > > production and algae based " Living fuel cell" technology", 
and
> > > > referred list members to his website for further information.
> > > > www.dabney.com/ecogenics/
> > > >
> > > > I didn't find much information there, maybe I should have 
looked
> > > > harder. I saw some photographs that looked to me like water
> > >hyacinth
> > > > and duckweed, nice for greywater/blackwater treatment 
systems. I
> > > > guess there's something I'm missing. I'm not being sceptical, 
> just
> > > > need more info I think. What's not clear to me is whether 
Marc 
> has
> > > > actually succeeded in producing lipids from algae in usable 
form
> > >and
> > > > quantity. When last we heard Marc hadn't made any biodiesel 
yet 
> but
> > > > would be doing so soon. I don't know if Marc has made yet 
> biodiesel
> > > > from algae lipids. Can you tell us a bit more Marc?
> > > >
> > > > Meanwhile, personally I take your view Lowell, cheap sources 
of 
> oil
> > > > seeds are more interesting. There's huge and very largely
> > >unexplored
> > > > potential in oil-bearing plants, as well as in productive and
> > > > efficient ways of producing them. For instance, a quick 
search 
> of
> > > > James Duke's Handbook of Energy Crops finds 62 legumes, both 
> plants
> > > > and trees, either of which can be fitted to the cropping and
> > >growing
> > > > patterns on integrated sutainable farms in a variety of ways,
> > >perhaps
> > > > as cover crops, interplanted or undersown, for forage or green
> > > > manure, earning their keep independently of their oil 
potential,
> > > > which would come as a bonus produced without the dedicated 
use 
> of
> > >of
> > > > any land, or time and labour. Trees can be even more 
> interesting.
> > > > That's just some of the legumes.
> > > >
> > > > http://www.hort.purdue.edu/newcrop/duke_energy/dukeindex.html
> > > > Handbook of Energy Crops Index
> > > >
> > > > Best
> > > >
> > > > Keith
> > > >
> > > >
> > > > >Lowell
> > > > >
> > > > >>From: "balaji" <[EMAIL PROTECTED]>
> > > > >>Reply-To: biofuel@yahoogroups.com
> > > > >>To: <biofuel@yahoogroups.com>
> > > > >>Subject: Re: [biofuel] Re: oil from algae...
> > > > >>Date: Sat, 1 May 2004 19:48:23 +0530
> > > > >>
> > > > >>Hi all,
> > > > >>So am I.
> > > > >>Balaji,
> > > > >>Chennai, TN, India
> > > > >>
> > > > >>----- Original Message -----
> > > > >>From: "Pieter Koole" <[EMAIL PROTECTED]>
> > > > >>To: <biofuel@yahoogroups.com>
> > > > >>Sent: Wednesday, April 28, 2004 1:26 AM
> > > > >>Subject: Re: [biofuel] Re: oil from algae...
> > > > >>
> > > > >>
> > > > >> > I am interested as well.
> > > > >> >
> > > > >> > Met vriendelijke groet,
> > > > >> > Pieter Koole
> > > > >> > Netherlands.
> > > > >> >
> > > > >> >
> > > > >> >
> > > > >> > The information contained in this message (including
> > >attachments) is
> > > > >> > confidential, and is intended for the addressee(s)
> > > > >> > only. If you have received this message in error please 
> delete
> > >it and
> > > > >> > notify the originator immediately. The unauthorized use,
> > >disclosure,
> > > > >> > copying or alteration of this message is strictly 
> forbidden.
> > >We will not
> > > > >>be
> > > > >> > liable for direct, special, indirect or
> > > > >> > consequential damages arising from alteration of the 
> contents
> > >of this
> > > > >> > message by a third party or in case of electronic
> > >communications as a
> > > > >>result
> > > > >> > of any virus being passed on.
> > > > >> >
> > > > >> >
> > > > >> > ----- Original Message -----
> > > > >> > From: "wwschnabel" <[EMAIL PROTECTED]>
> > > > >> > To: <biofuel@yahoogroups.com>
> > > > >> > Sent: Tuesday, April 27, 2004 4:42 AM
> > > > >> > Subject: Re: [biofuel] Re: oil from algae...
> > > > >> >
> > > > >> >
> > > > >> > > I asked a while ago if anyone had any info on Oil from 
> algae.
> > > > >> > >
> > > > >> > > What I would like to do is an experiment.
> > > > >> > >
> > > > >> > > Does anyone have any info on how exactly to extract 
the 
> oil
> > >from
> > > > >>algae?
> > > > >> > Could I do it in a home lab?
> > > > >> > >
> > > > >> > > Thanks,
> > > > >> > >
> > > > >> > > Bill




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