Hello Paul.
It seems to me that you produced some soap that time. Did you measure the
FFA content before starting ?
Best regards
Jan Warnqvist
AGERATEC AB

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----- Original Message ----- 
From: "Paul Tanner" <[EMAIL PROTECTED]>
To: <[EMAIL PROTECTED]>
Sent: Wednesday, March 30, 2005 1:00 AM
Subject: [Biofuel] liquid glycerine


>
>
>
>
> Hi,
>
> I've been making Biodiesel (BD) for a few months, now.. using the Mike
> Pelly method.. and a curious thing happened with the last batch (my
batches
> are in approx. 160 - 180 litres).. the glycerine was liquid after the
> reaction. This is the first time this has occurred for me, all other times
> the glycerine formed and settle in my tank, and was solid at low
> temperatures.
>
> I had measured accurately, the quantities of methanol, caustic soda and
> volume of oil...( I had an interested observer, who can testify if
> required!! :-)  ) I watched the colour of the mixture change, as I was
> agitating, from a light caramel colour to a dark molasses colour... then
> observed the glycerine start to settle, as expected. At this time the
> glycerine was quite warm, so was still liquid, however, I let the mixture
> settle for a 2 week period and the glycerine has not set firm. maybe I
> should not complain.. 'cos it was easy to drain out of the tank! :-)
>
> Did the reaction not go far enough?  Any further ideas on what has
> happened??
>
> regards,
>
> Paul.
> -------------------------------------------
> Paul Tanner
> Software IT Architect
> Melbourne, Australia
>
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