my problem is emulsion.. i guess just just have to practice a few more
times, and also allow longer reaction time (more than 24 hrs) before
washing..

Thanks,

On 1/9/07, Tonomár András <[EMAIL PROTECTED]> wrote:
> What is your real problem?
> Yre you getting emulsion? or draining problem?
> Andrew
>
>
>
>
> Hey Andrew,
>
> Thanks for the info and advice..
>
> I will work harder..
>
>
> On 1/8/07, Tonomár András <[EMAIL PROTECTED]> wrote:
> > Hello Joe,
> >
> > My experience is that I get about 96%-100% yield for the whole process.
> > In your terms 100ml VWO - 96ml finished BD
> > I wash 5 times stirring with a paint stirrer.
> > If you are carefull then you dont use BD during the wash. (at least you
> > should not)
> > What you loose is contaminents like soaps, exess methanol, free glycerin
> > etc.
> >
> > The best advise to say for you is to practice, and info will come.
> > This you can read about for hours, but without doing it you will never
> > learn.
> >
> > Everyone makes mistakes, that is how we learn.
> >
> > Email if you have questions.
> > Andrew
> >
> >
> >
> >
> > > Hi guys,
> > >
> > > If i use, say, 100ml of BD and add 50 ml of hot water for washing
> > > (stir for 15 mins), will i get back 100ml of washed BD or less?
> > >
> > > Thanks,
> > > Joe N.
> > >
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