Hi Charles,
Thank you. Both approaches make sense, and I think I will give the gyroA
method a go.
And yes, the advisory is appreciated and one I've considered. Luckily, I'm
looking at a metalloprotein (no tag flexibility) and the tensors derived
independently from RDCs and PCSs found a Xax within 0.5 (*10^-32 m^3). So
the approximation of a single tensor isn't unreasonable in this case, I
think.
Best,
John

On Wed, May 6, 2020 at 4:43 PM Charles Schwieters <[email protected]>
wrote:

>
> Hello John--
> >
>
> > I'm looking to perform a refinement with a combination of PCSs and
> > paramagnetic induced RDCs. Ideally, I would like to use a single
> tensor object
> > to describe them (i.e. have the Xax, Xrh, Euler Angles shared between
> PCSs and
> > RDCs)
> >
> > If I write something as shown below, the Da would be properly set for PCS
> > refinement... but this would be much too large for the RDC restraints.
> > The relationship between Xax and Da should be something as follows:
> > Dax = ((Xax)/(30*u0*k*T))*(Bo**2*39.46)
>
> *If* the alignment tensors are indeed the same aside from scaling, you
> can set this factor using the gyroA member of RDCPot, either the one
> corresponding to PCS data, or the one for RDC data, e.g.
>
> for M in Metals:
>     Para_Pot = PotList('Para_{}'.format(M))
>     Restraint = '{0}_NH_PCSs'.format(M)
>     PCS_File = 'PCS_tbl_Files/{0}_NH_PCSs.tbl'.format(M)
>     pcs_restr = create_RDCPot(Restraint, PCS_File, Metal_Tensors[M])
>     pcs_restr.setUseDistance(True)
>     pcs_restr.setGyroA( FACTOR )
>     ...
>
> However, as my colleague Guillermo Bermejo points out:
>
>   I think it might be relevant to ask whether there's motion involved
>   in the paramagnet (e.g., flexible tag). If so, I believe the
>   effective tensor involved in the PCS and RDC data might be
>   different, because the two types of data average differently, so
>   forcing the same tensor on both datasets may not be the right way to
>   go.
>
> It is also possible to set as the same the orientation and rhombicity
> of two different tensors - allowing the Da only to vary. There's an
> example of this approach in eginput/dna_refi/ensemble.py in the
> Xplor-NIH distribution.
>
> best regards--
> Charles
>


-- 
*John B. Stiller*
Ph.D. Candidate
Kern Group
Department of Biochemistry
Brandeis University

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