Hi Celia,

I have waited Charles's response because he always brings something new to
the community that I might not catch up with well. If you are working on
NMRFAM-Sparky, you can try two-letter-code "c3" first that will automate
NOESY assignments, TALOS-N and Xplor-NIH calculation. You can customize the
generated Xplor-NIH scripts after the initial run.

Cheers,
Woonghee


On Fri, May 8, 2020 at 11:04 AM Charles Schwieters <[email protected]>
wrote:

> Hello Celia--
>
> It seems that it took 3 days for your email to cross the Straights of
> Florida. That's a pity.
>
> > I am calculating the structure of a protein with Sparky. I already
> > have NOE restrictions, but I also want to introduce proton chemical
> > shift restrains.
>
> When using Xplor-NIH, most commonly, or at least as a first step,
> chemical shift values are used to generate torsion-angle restraints
> using the program Talos-N (
> https://spin.niddk.nih.gov/bax/software/TALOS-N/).
> The restraints are then used along with distance restraints in initial
> structure determination. A simple script for an initial calculation
> can be found in the file xplor-nih-tutorial-2018/gb1_simple/fold_nordc.py
> in this link: http://nmr.cit.nih.gov/xplor-nih/xplor-nih-tutorial.tgz
>
> Xplor-NIH also has a few explicit energy terms which can be used to
> refine directly against chemical shifts, including SpartaPot (based on
> Sparta) and CSPot (based on the CamShift algorithm), but I would first
> start with the standard approach for structure-determination in the
> above-mentioned fold script.
>
> best regards--
> Charles
>
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-- 
================================================

*Woonghee Lee, I.E.I.P., M.S., Ph.D.*

Assistant Scientist
        and
Principal Investigator

National Magnetic Resonance Facility at Madison (NMRFAM)
and Biochemistry Department
University of Wisconsin-Madison
DeLuca Biochemistry Laboratories
433 Babcock Drive Rm B160E
Madison, WI USA 53706-1544
[email protected], [email protected]
Office: +1-608-263-1722
https://sites.google.com/view/wlee-group
www.nmrfam.wisc.edu

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