Matheus A couple of points Firstly, isn't this pseudo merohedral rather than merohedral. I realise you didn't mention either in your email but it is in the title of the previous message.
Secondly, the difference in the cell dimensions (b=123.92 and c=128.89A) appears to be quite large and should lead to split spots which (I think) corresponds to non merohedral twinning. Did you observe these but integrated them as one? My main interest in this is whether, with a high resolution set up (low divergence beam and high resolution detector), the individual contributions could be separated out. Secondly whether it would be useful to do so e.g. for the case where the twin fraction is near 50% Regards Colin (Regarding what to call the twinning I have some sympathies with Humpty Dumpty's view "When I use a word... it means just what I choose it to mean-neither more nor less" As important a philosopher as Wittgenstein.) ________________________________ From: CCP4 bulletin board [mailto:ccp...@jiscmail.ac.uk] On Behalf Of Matheus Pinheiro Sent: 22 June 2010 12:00 To: CCP4BB@JISCMAIL.AC.UK Subject: Re: [ccp4bb] Merohedral twining for P212121. Hi Yang, I had the experience to work with twinning in P212121 space group. My crystals belong to space group P212121 with unit cell dimensions a=82.39, b=123.92 and c=128.89A. You can see that "b" and "c" are not equal but very simmilar, and this fact can allow twinning for this space group. The crystals with higher fraction of twinning can be easier processed in tetragonal space group P41212 with unit cell dimensions a=b=126.95 and c=82.43A. However the packing is actually orthorhombic. In my work, to fully assess the twin fraction and the twin operator was employed the program PHENIX (xtriage tool). I solved my crystal structure using data suggested by PHENIX program (twin operator (-h,-l,-k)). Good luck! Matheus On Mon, 21 Jun 2010 13:52:05 -0700, yang li wrote > Dear all, > > Is there any possible of twining for a normal P212121 spacegroup and what is the twin law, say no equal cell dimensions? > Some people said there is no twin law for such symmetry but I am not very sure. Thanks a lot. > > Best > Yang ------------------------------------------------------------- Matheus Pinto Pinheiro Laboratório de Cristalografia de Proteínas Departamento de Física e Química Faculdade de Ciências Farmacêuticas de Ribeirão Preto - USP Brasil Fone: +55.16.3602.4193 m...@fcfrp.usp.br