Hi, Did you use detergent? It seems look like detergent crystals.

2010-08-25 



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发件人: rui 
发送时间: 2010-08-25  20:37:18 
收件人: CCP4BB 
抄送: 
主题: [ccp4bb] turn granular to crystal 
 
Hi, All,

I'm trying to crystallize a soluble protein and got something like granular, 
they are rounded shaped and not so regular and also don't have sharp edges. See 
the attached pic. The current condition is PEG4000 and pH around 5. How can I 
improve this condition? Thanks a lot.

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