[biofuel] New Distillers FAQ

2004-01-29 Thread Ackland, Tony (CALNZAS)

x-charset ISO-8859-1NEW DISTILLERS Frequently Asked Questions (Feb'03) 

Posted near the 1st of each month, to the NEW_DISTILLERS newsgroup at 
www.yahoogroups.com 

Please email any additions, corrections, clarifications required, etc regarding 
the FAQ to Tony Ackland ([EMAIL PROTECTED]), however please direct any general 
questions to the newsgroup itself. 

*** 

1) Is distilling hard to do ? 
2) Is it legal ? 
3) Will it make me blind ? 
4) Whats the difference between a pot still, reflux still, and fractionating 
column ? 
5) How do I get or make a still ? 
6) How do I make a whisky / rum / vodka / gin ? 
7) Should I use sugar or grains ? 
8) Can I use fruit wine ? 
9) How do I make a Turbo-all-sugar wash ? 
10) How do I run a Pot still ? 
11) How do I run a Reflux still ? 
12) Can I use a reflux still to make rum or whisky ? 
13) How do I measure the strength of it  dilute it ? 
14) How do I get rid of that off-taste ? 
15) Why do my spirits turn cloudy when diluted ? 
16) How do I flavour/turn the vodka's into something else ? 
17) What web resources are there ? 
18) How do I contact the NEW DISTILLERS news group ? 
19) Can I run my car on it ? 
20) How do I convert between gallons and litres and  
21) What is a Thumper ? 
22) Can methylated spirits be made safe to drink ? 

** 

1) Is distilling hard to do ?

Nope - if you can follow instructions enough to bake scones, then you can 
sucessfully distil. To distil well however, will require you to understand what 
you're doing, so read around and get a bit of information under your belt 
before you begin. 

2) Is it legal ?

Probably not. It is only legal in New Zealand, and some European countries turn 
a blind eye to it, but elsewhere it is illegal, with punishment ranging from 
fines to imprisonment or floggings. This action against it is usually the 
result of either religous beliefs (right or wrong), but more generally due to 
the great revenue base it provides Governements through excise taxes. So if you 
are going to distil, just be aware of the potential legal ramifications. 

3) Will it make me blind ?

Not if you're careful. This pervasive question is due to moonshine lore, which 
abounds with myths of blindness, but few actual documented cases. The concern 
is due to the presence of methanol (wood alcohol), an optic nerve poison, which 
can be present in small amounts when fermenting grains or fruits high in 
pectin. This methanol comes off first from the still, so it is easily 
segregated and discarded, and easily observed via changes in the vapour 
temperature. A simple rule of thumb for this is to throw away the first 50 mL 
you collect (per 20 L mash used). Probably the greatest risk to your health 
during distilling is the risk of fire - collecting a flammable liquid near a 
heat source. So keep a fire extinguisher nearby. 

The cases where you do hear about people poisoned by illict spirits have been 
the terrible situations where adulterants such as methanol, antifreeze, battery 
acid etc have been added to the spirits afterwards by unscrupulous sellers (for 
what misguided reasons ??). If you have had a healthy fermentation take place, 
it is infact very difficult to make methanol. The other problems have been lead 
poisoning when people have used lead-based products (ie lead solder) when 
constructing their still, instead of something more appropriate for food-grade 
vessels. The rules should infact be dont buy spirits from an unknown supplier 
- but its very safe to distill for yourself. 

4) Whats the difference between a pot still, reflux still, and fractionating 
column ?

A pot still simply collects and condenses the alcohol vapours that come off the 
boiling mash. This will result in an alcohol at about 40-60% purity, with 
plenty of flavour in it. If this distillate were put through the pot still 
again, it would increase in purity to around 70-85% purity, and lose a bit of 
its flavour. 

A reflux still does these multiple distillations in one single go, by having 
some packing in a column between the condensor  the pot, and allowing some of 
the vapour to condense and trickle back down through the packing. This reflux 
of liquid helps clean the rising vapour and increase the % purity. The taller 
the packed column, and the more reflux liquid, the purer the product will be. 
The advantage of doing this is that it will result in a clean vodka, with 
little flavour to it - ideal for mixing with flavours etc. 

A fractionating column is a pure form of the reflux still. It will condense all 
the vapour at the top of the packing, and return about 9/10 back down the 
column. The column will be quite tall - say 600-1200mm (2-4 foot), and packed 
with a material high in surface area, but which takes up little space (pot 
scrubbers are good for this). It will result in an alcohol 95%+ pure (the 

[biofuel] New Distillers Frequently Asked Questions (FAQ)

2003-11-02 Thread Ackland, Tony (CALNZAS)

NEW DISTILLERS Frequently Asked Questions (last modified Feb'03) 

Posted near the 1st of each month, to the NEW_DISTILLERS newsgroup at 
www.yahoogroups.com 

Please email any additions, corrections, clarifications required, etc regarding 
the FAQ to Tony Ackland ([EMAIL PROTECTED]), however please direct any general 
questions to the newsgroup itself. 

*** 

1) Is distilling hard to do ? 
2) Is it legal ? 
3) Will it make me blind ? 
4) Whats the difference between a pot still, reflux still, and fractionating 
column ? 
5) How do I get or make a still ? 
6) How do I make a whisky / rum / vodka / gin ? 
7) Should I use sugar or grains ? 
8) Can I use fruit wine ? 
9) How do I make a Turbo-all-sugar wash ? 
10) How do I run a Pot still ? 
11) How do I run a Reflux still ? 
12) Can I use a reflux still to make rum or whisky ? 
13) How do I measure the strength of it  dilute it ? 
14) How do I get rid of that off-taste ? 
15) Why do my spirits turn cloudy when diluted ? 
16) How do I flavour/turn the vodka's into something else ? 
17) What web resources are there ? 
18) How do I contact the NEW DISTILLERS news group ? 
19) Can I run my car on it ? 
20) How do I convert between gallons and litres and  
21) What is a Thumper ? 
22) Can methylated spirits be made safe to drink ? 

** 

1) Is distilling hard to do ?

Nope - if you can follow instructions enough to bake scones, then you can 
sucessfully distil. To distil well however, will require you to understand what 
you're doing, so read around and get a bit of information under your belt 
before you begin. 

2) Is it legal ?

Probably not. It is only legal in New Zealand, and some European countries turn 
a blind eye to it, but elsewhere it is illegal, with punishment ranging from 
fines to imprisonment or floggings. This action against it is usually the 
result of either religous beliefs (right or wrong), but more generally due to 
the great revenue base it provides Governements through excise taxes. So if you 
are going to distil, just be aware of the potential legal ramifications. 

3) Will it make me blind ?

Not if you're careful. This pervasive question is due to moonshine lore, which 
abounds with myths of blindness, but few actual documented cases. The concern 
is due to the presence of methanol (wood alcohol), an optic nerve poison, which 
can be present in small amounts when fermenting grains or fruits high in 
pectin. This methanol comes off first from the still, so it is easily 
segregated and discarded, and easily observed via changes in the vapour 
temperature. A simple rule of thumb for this is to throw away the first 50 mL 
you collect (per 20 L mash used). Probably the greatest risk to your health 
during distilling is the risk of fire - collecting a flammable liquid near a 
heat source. So keep a fire extinguisher nearby. 

The cases where you do hear about people poisoned by illict spirits have been 
the terrible situations where adulterants such as methanol, antifreeze, battery 
acid etc have been added to the spirits afterwards by unscrupulous sellers (for 
what misguided reasons ??). If you have had a healthy fermentation take place, 
it is infact very difficult to make methanol. The other problems have been lead 
poisoning when people have used lead-based products (ie lead solder) when 
constructing their still, instead of something more appropriate for food-grade 
vessels. The rules should infact be dont buy spirits from an unknown supplier 
- but its very safe to distill for yourself. 

4) Whats the difference between a pot still, reflux still, and fractionating 
column ?

A pot still simply collects and condenses the alcohol vapours that come off the 
boiling mash. This will result in an alcohol at about 40-60% purity, with 
plenty of flavour in it. If this distillate were put through the pot still 
again, it would increase in purity to around 70-85% purity, and lose a bit of 
its flavour. 

A reflux still does these multiple distillations in one single go, by having 
some packing in a column between the condensor  the pot, and allowing some of 
the vapour to condense and trickle back down through the packing. This reflux 
of liquid helps clean the rising vapour and increase the % purity. The taller 
the packed column, and the more reflux liquid, the purer the product will be. 
The advantage of doing this is that it will result in a clean vodka, with 
little flavour to it - ideal for mixing with flavours etc. 

A fractionating column is a pure form of the reflux still. It will condense all 
the vapour at the top of the packing, and return about 9/10 back down the 
column. The column will be quite tall - say 600-1200mm (2-4 foot), and packed 
with a material high in surface area, but which takes up little space (pot 
scrubbers are good for this). It will result in an alcohol 95%+ pure (the 

[biofuel] NEW DISTILLERS Frequently Asked Questions

2003-07-29 Thread Ackland, Tony (CALNZAS)

NEW DISTILLERS Frequently Asked Questions (Feb'03) 

Posted near the 1st of each month, to the NEW_DISTILLERS newsgroup at 
www.yahoogroups.com 

Please email any additions, corrections, clarifications required, etc regarding 
the FAQ to Tony Ackland ([EMAIL PROTECTED]), however please direct any general 
questions to the newsgroup itself. 

*** 

1) Is distilling hard to do ? 
2) Is it legal ? 
3) Will it make me blind ? 
4) Whats the difference between a pot still, reflux still, and fractionating 
column ? 
5) How do I get or make a still ? 
6) How do I make a whisky / rum / vodka / gin ? 
7) Should I use sugar or grains ? 
8) Can I use fruit wine ? 
9) How do I make a Turbo-all-sugar wash ? 
10) How do I run a Pot still ? 
11) How do I run a Reflux still ? 
12) Can I use a reflux still to make rum or whisky ? 
13) How do I measure the strength of it  dilute it ? 
14) How do I get rid of that off-taste ? 
15) Why do my spirits turn cloudy when diluted ? 
16) How do I flavour/turn the vodka's into something else ? 
17) What web resources are there ? 
18) How do I contact the NEW DISTILLERS news group ? 
19) Can I run my car on it ? 
20) How do I convert between gallons and litres and  
21) What is a Thumper ? 
22) Can methylated spirits be made safe to drink ? 

** 
1) Is distilling hard to do ?
Nope - if you can follow instructions enough to bake scones, then you can 
sucessfully distil. To distil well however, will require you to understand what 
you're doing, so read around and get a bit of information under your belt 
before you begin. 
2) Is it legal ?
Probably not. It is only legal in New Zealand, and some European countries turn 
a blind eye to it, but elsewhere it is illegal, with punishment ranging from 
fines to imprisonment or floggings. This action against it is usually the 
result of either religous beliefs (right or wrong), but more generally due to 
the great revenue base it provides Governements through excise taxes. So if you 
are going to distil, just be aware of the potential legal ramifications. 
3) Will it make me blind ?
Not if you're careful. This pervasive question is due to moonshine lore, which 
abounds with myths of blindness, but few actual documented cases. The concern 
is due to the presence of methanol (wood alcohol), an optic nerve poison, which 
can be present in small amounts when fermenting grains or fruits high in 
pectin. This methanol comes off first from the still, so it is easily 
segregated and discarded, and easily observed via changes in the vapour 
temperature. A simple rule of thumb for this is to throw away the first 50 mL 
you collect (per 20 L mash used). Probably the greatest risk to your health 
during distilling is the risk of fire - collecting a flammable liquid near a 
heat source. So keep a fire extinguisher nearby. 

The cases where you do hear about people poisoned by illict spirits have been 
the terrible situations where adulterants such as methanol, antifreeze, battery 
acid etc have been added to the spirits afterwards by unscrupulous sellers (for 
what misguided reasons ??). If you have had a healthy fermentation take place, 
it is infact very difficult to make methanol. The other problems have been lead 
poisoning when people have used lead-based products (ie lead solder) when 
constructing their still, instead of something more appropriate for food-grade 
vessels. The rules should infact be dont buy spirits from an unknown supplier 
- but its very safe to distill for yourself. 
4) Whats the difference between a pot still, reflux still, and fractionating 
column ?
A pot still simply collects and condenses the alcohol vapours that come off the 
boiling mash. This will result in an alcohol at about 40-60% purity, with 
plenty of flavour in it. If this distillate were put through the pot still 
again, it would increase in purity to around 70-85% purity, and lose a bit of 
its flavour. 

A reflux still does these multiple distillations in one single go, by having 
some packing in a column between the condensor  the pot, and allowing some of 
the vapour to condense and trickle back down through the packing. This reflux 
of liquid helps clean the rising vapour and increase the % purity. The taller 
the packed column, and the more reflux liquid, the purer the product will be. 
The advantage of doing this is that it will result in a clean vodka, with 
little flavour to it - ideal for mixing with flavours etc. 

A fractionating column is a pure form of the reflux still. It will condense all 
the vapour at the top of the packing, and return about 9/10 back down the 
column. The column will be quite tall - say 600-1200mm (2-4 foot), and packed 
with a material high in surface area, but which takes up little space (pot 
scrubbers are good for this). It will result in an alcohol 95%+ pure (the 
theoretical limit without 

[biofuel] Re Ethanol from bread waste?

2003-06-11 Thread Ackland, Tony (CALNZAS)

Gary,

 I can't seem to get this link to work - any ideas?
 http://homedistiller.org/wash-grain2.htm#bread 

works OK for me. 

Tony

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[biofuel] Re Ethanol from bread waste?

2003-06-09 Thread Ackland, Tony (CALNZAS)

Bread has been used in the production of vodka before, basically as a source of 
the starch.  See http://homedistiller.org/wash-grain2.htm#bread for more 
details.

Tony

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[biofuel] Re: Biogas from chicken manure

2003-06-01 Thread Ackland, Tony (CALNZAS)

thanks Keith  Peter.  Doing the research for a friend of my fathers, so I may 
be back later with more questions once he's had a chance to work through all 
those links.

Tony

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[biofuel] Biogas from chicken manure

2003-05-29 Thread Ackland, Tony (CALNZAS)

Does anyone have pointers re producing biogas / methane from chicken manure, 
and its subsequent use in firing heaters for nurseries ?

Tony

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[biofuel] Re: New Distillers FAQ

2003-05-21 Thread Ackland, Tony (CALNZAS)

*poink* well, that was a load of BS.  no documented cases?  what about the 2 
or 3 dozen people killed in a single incident in China a year or so ago?

Paul - could you please give me a few more leads about what happened there ?  

Of the cases I have heard of, poisoning from illict spirits has only been due 
to other contaminants being mixed into either the brew before distilling, or 
added as adulterants afterwards.  Antifreeze and methanol being the common 
culprits (they're all alcohol aren't they ??).  Not recommended behavour.  
Those are the practices of unscruplous sellers, not a home-distiller making for 
personal consumption.   The point maybe to make is dont buy alcohol from an 
illicit seller who you dont know, not dont distill yourself.

Adding adulterants is not the same as making up your own safe brew with a clean 
fermentation and basic housekeeping guidelines that any brewer knows. Its quite 
hard to actually make methanol via fermentation of sugar or grains.

The only other problems I'm aware of is when lead-soldered condensers have been 
used (ie http://www.cdc.gov/mmwr/preview/mmwrhtml/00016616.htm ) - hence the 
need for education around safe practices, materials, etc and again, not 
something that you're likely to do to yourself, particularly if you have read 
the guidelines.

No - you dont need a well equiped lab.  More a matter of understanding clearly 
what you're doing, and why.  Read around - there is now quality information 
available on the subject (as pointed out in the FAQ)

Tony



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[biofuel] New Distillers FAQ

2003-05-20 Thread Ackland, Tony (CALNZAS)

 NEW DISTILLERS Frequently Asked Questions (Feb'03) 
 
 Posted near the 1st of each month, to the NEW_DISTILLERS newsgroup at 
 www.yahoogroups.com 
 
 Please email any additions, corrections, clarifications required, etc 
 regarding the FAQ to Tony Ackland ([EMAIL PROTECTED]), however please direct 
 any general questions to the newsgroup itself. 
 
 *** 
 
 1) Is distilling hard to do ? 
 2) Is it legal ? 
 3) Will it make me blind ? 
 4) Whats the difference between a pot still, reflux still, and fractionating 
 column ? 
 5) How do I get or make a still ? 
 6) How do I make a whisky / rum / vodka / gin ? 
 7) Should I use sugar or grains ? 
 8) Can I use fruit wine ? 
 9) How do I make a Turbo-all-sugar wash ? 
 10) How do I run a Pot still ? 
 11) How do I run a Reflux still ? 
 12) Can I use a reflux still to make rum or whisky ? 
 13) How do I measure the strength of it  dilute it ? 
 14) How do I get rid of that off-taste ? 
 15) Why do my spirits turn cloudy when diluted ? 
 16) How do I flavour/turn the vodka's into something else ? 
 17) What web resources are there ? 
 18) How do I contact the NEW DISTILLERS news group ? 
 19) Can I run my car on it ? 
 20) How do I convert between gallons and litres and  
 21) What is a Thumper ? 
 22) Can methylated spirits be made safe to drink ? 
 
 ** 
 
 1) Is distilling hard to do ?
 
 Nope - if you can follow instructions enough to bake scones, then you can 
 sucessfully distil. To distil well however, will require you to understand 
 what you're doing, so read around and get a bit of information under your 
 belt before you begin. 
 
 2) Is it legal ?
 
 Probably not. It is only legal in New Zealand, and some European countries 
 turn a blind eye to it, but elsewhere it is illegal, with punishment ranging 
 from fines to imprisonment or floggings. This action against it is usually 
 the result of either religous beliefs (right or wrong), but more generally 
 due to the great revenue base it provides Governements through excise taxes. 
 So if you are going to distil, just be aware of the potential legal 
 ramifications. 
 
 3) Will it make me blind ?
 
 Not if you're careful. This pervasive question is due to moonshine lore, 
 which abounds with myths of blindness, but few actual documented cases. The 
 concern is due to the presence of methanol (wood alcohol), an optic nerve 
 poison, which can be present in small amounts when fermenting grains or 
 fruits high in pectin. This methanol comes off first from the still, so it is 
 easily segregated and discarded. A simple rule of thumb for this is to throw 
 away the first 50 mL you collect (per 20 L mash used). Probably the greatest 
 risk to your health during distilling is the risk of fire - collecting a 
 flammable liquid near a heat source. So keep a fire extinguisher nearby. 
 
 4) Whats the difference between a pot still, reflux still, and fractionating 
 column ?
 
 A pot still simply collects and condenses the alcohol vapours that come off 
 the boiling mash. This will result in an alcohol at about 40-60% purity, with 
 plenty of flavour in it. If this distillate were put through the pot still 
 again, it would increase in purity to around 70-85% purity, and lose a bit of 
 its flavour. 
 
 A reflux still does these multiple distillations in one single go, by having 
 some packing in a column between the condensor  the pot, and allowing some 
 of the vapour to condense and trickle back down through the packing. This 
 reflux of liquid helps clean the rising vapour and increase the % purity. 
 The taller the packed column, and the more reflux liquid, the purer the 
 product will be. The advantage of doing this is that it will result in a 
 clean vodka, with little flavour to it - ideal for mixing with flavours etc. 
  
 
 A fractionating column is a pure form of the reflux still. It will condense 
 all the vapour at the top of the packing, and return about 9/10 back down the 
 column. The column will be quite tall - say 600-1200mm (2-4 foot), and packed 
 with a material high in surface area, but which takes up little space (pot 
 scrubbers are good for this). It will result in an alcohol 95%+ pure (the 
 theoretical limit without using a vacuum is 96.48 %(by volume)), with no 
 other tastes or impurities in it. 
 
 5) How do I get or make a still ?
 
 If you're after a pot still, these are generally home made using what-ever 
 you have at hand - say copper tubing and old water heaters or pressure 
 cookers. You don't really need any plans for these - just follow any of the 
 photos about. 
 
 Reflux stills can be made from plans on the net, or bought from several 
 manufacturers. For reflux still plans see
 The photos section at http://homedistiller.org/photos-ns.htm for Offset 
 head designs, and http://homedistiller.org/photos-reflux.htm for general 
 reflux 

[biofuel] Language

2003-04-06 Thread Ackland, Tony (CALNZAS)

Guys,

Could you please keep the use of profanities down to a minimum.  My companies 
email virus filter blocks also based on inappropriate content, and this means 
that I get to lose the whole days digest of emails just because some idiot 
can't express himself clearly enough without swearing.

Tony

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[biofuel] RE: Methanol .. was IS BUSH NUTS?

2003-02-26 Thread Ackland, Tony (CALNZAS)

The soda - aspartame-methanol toxicity link has been discounted many times - 
the concentrations are far too low.  See 
http://www.urbanlegends.com/ulz/nutrasweet.html It comes down to your ability 
to swill 375 cans of soda in a couple of hours.  

Tony

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[biofuels-biz] [Distillers] 1984 Orwell style

2002-04-04 Thread Ackland, Tony (CALNZAS)

 From one of our members ...
*

 

About one month ago, I had someone ring my doorbell. When I answered, I was
met by 2 men displaying badges and identifying themselves as agents of the
state tax department. They asked if they could talk to me for a minute, to
which I consented.
They had a folder, with my name on it, which they referred to. They said
they had information that I had bought a distillation device
 From a company in Canada. I had not bought anything from Canada, but had
bought a ss still from a company in the US on E-bay. I HAD requested
information from the Canadian company, but didn't buy anything.
To make a long story short, they wanted to know where the device was now.
I told them I had sold it to someone in another state 3 years ago as it
didn't distill water fast enough.
They told me that they had to track down all stills that might be used
to produce alcohol without a permit.
I find this totally incomprehensible that a state agency would spend the
money to investigate a still purchase that could produce such a small amount

of alcohol. They seemed to be satisfied and left..Keep wondering if they
will be back with a warrant.
I would like to really pursue this, but I don't want to call any further
attention to myself. Ridiculous.
Bottom line===BE CAREFUL.


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[biofuel] [Distillers] 1984 Orwell style

2002-04-04 Thread Ackland, Tony (CALNZAS)

 From one of our members ...
*

 

About one month ago, I had someone ring my doorbell. When I answered, I was
met by 2 men displaying badges and identifying themselves as agents of the
state tax department. They asked if they could talk to me for a minute, to
which I consented.
They had a folder, with my name on it, which they referred to. They said
they had information that I had bought a distillation device
 From a company in Canada. I had not bought anything from Canada, but had
bought a ss still from a company in the US on E-bay. I HAD requested
information from the Canadian company, but didn't buy anything.
To make a long story short, they wanted to know where the device was now.
I told them I had sold it to someone in another state 3 years ago as it
didn't distill water fast enough.
They told me that they had to track down all stills that might be used
to produce alcohol without a permit.
I find this totally incomprehensible that a state agency would spend the
money to investigate a still purchase that could produce such a small amount

of alcohol. They seemed to be satisfied and left..Keep wondering if they
will be back with a warrant.
I would like to really pursue this, but I don't want to call any further
attention to myself. Ridiculous.
Bottom line===BE CAREFUL.


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[biofuel] Kiwi_Distiller moving on ..

2002-03-03 Thread Ackland, Tony (CALNZAS)

Guys  Gals,

Just a couple of months pre-warning here.  

Most of you are fairly aware that my Distilling site has already moved
FROM   http://www.geocities.com/kiwi_distiller 
TOhttp://homedistiller.org  

(along with a mirror at http://distiller.servebeer.com ) - with a great big 
thanks to Dave  DC for letting me use their server space.

I've kept the kiwi_distiller site running  up to date in the background 
anyhow.  
Well, Geocities have turned up the pressure, and are now making that harder to 
do.  As from April, I'll close the kiwi_distiller site, and only maintain the 
homedistiller and servebeer sites.   

Thanks for your patronage at the old site, and don't forget to update your 
bookmarks to the new one.

cheers

Tony
http://homedistiller.org


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[biofuel] Blueflame text

2001-12-16 Thread Ackland, Tony (CALNZAS)

Ken,

I've got an HTML version of it on my site.  See
http:\\homedistiller.org\blueflame.htm

Tony
http:\\homedistiller.org


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[biofuel] New Distillers FAQ

2001-11-18 Thread Ackland, Tony (CALNZAS)

NEW DISTILLERS Frequently Asked Questions (Sept'01) 

Posted near the 1st of each month, to the NEW_DISTILLERS newsgroup at
www.yahoogroups.com 

Please email any additions, corrections, clarifications required, etc
regarding the FAQ to Tony Ackland ([EMAIL PROTECTED]), however please
direct any general questions to the newsgroup itself. 

*** 

1) Is distilling hard to do ? 
2) Is it legal ? 
3) Will it make me blind ? 
4) Whats the difference between a pot still, reflux still, and fractionating
column ? 
5) How do I get or make a still ? 
6) How do I make a whisky / rum / vodka / gin ? 
7) Should I use sugar or grains ? 
8) Can I use fruit wine ? 
9) How do I get rid of that off-taste ? 
10) How do I measure the strength of it  dilute it ? 
11) How do I flavour/turn the vodka's into something else ? 
12) What web resources are there ? 
13) How do I contact the NEW DISTILLERS news group ? 
14) Can I run my car on it ? 
15) How do I convert between gallons and litres and  
16) What is a Thumper ? 
17) Can I use a reflux still to make rum or whisky ? 

** 

1) Is distilling hard to do ?

Nope - if you can follow instructions enough to bake scones, then you can
sucessfully distil. To distil well however, will require you to understand
what you're doing, so read around and get a bit of information under your
belt before you begin. 

2) Is it legal ?

Probably not. It is only legal in New Zealand, and some European countries
turn a blind eye to it, but elsewhere it is illegal, with punishment ranging
from fines to imprisonment or floggings. This action against it is usually
the result of either religous beliefs (right or wrong), but more generally
due to the great revenue base it provides Governements through excise taxes.
So if you are going to distil, just be aware of the potential legal
ramifications. 

3) Will it make me blind ?

Not if you're careful. This pervasive question is due to moonshine lore,
which abounds with myths of blindness, but few actual documented cases. The
concern is due to the presence of methanol (wood alcohol), an optic nerve
poison, which can be present in small amounts when fermenting grains or
fruits high in pectin. This methanol comes off first from the still, so it
is easily segregated and discarded. A simple rule of thumb for this is to
throw away the first 50 mL you collect (per 20 L mash used). Probably the
greatest risk to your health during distilling is the risk of fire -
collecting a flammable liquid near a heat source. So keep a fire
extinguisher nearby. 

4) Whats the difference between a pot still, reflux still, and fractionating
column ?

A pot still simply collects and condenses the alcohol vapours that come off
the boiling mash. This will result in an alcohol at about 40-60% purity,
with plenty of flavour in it. If this distillate were put through the pot
still again, it would increase in purity to around 70-85% purity, and lose a
bit of its flavour. 

A reflux still does these multiple distillations in one single go, by having
some packing in a column between the condensor  the pot, and allowing some
of the vapour to condense and trickle back down through the packing. This
reflux of liquid helps clean the rising vapour and increase the % purity.
The taller the packed column, and the more reflux liquid, the purer the
product will be. The advantage of doing this is that it will result in a
clean vodka, with little flavour to it - ideal for mixing with flavours etc.


A fractionating column is a pure form of the reflux still. It will condense
all the vapour at the top of the packing, and return about 9/10 back down
the column. The column will be quite tall - say 600-1200mm (2-4 foot), and
packed with a material high in surface area, but which takes up little space
(pot scrubbers are good for this). It will result in an alcohol 95%+ pure
(the theoretical limit without using a vacuum is 96.48 %(by volume)), with
no other tastes or impurities in it. 

5) How do I get or make a still ?

If you're after a pot still, these are generally home made using what-ever
you have at hand - say copper tubing and old water heaters or pressure
cookers. Reflux stills can be made from plans on the net, or bought from
several manufacturers. For reflux stil plans see Stillmakers Build a World
Class Distillation Apparatus at http://www.Moonshine-Still.com (Free!) or
Gert Strands : http://partyman.se/Engelsk/default.htm (US$5). A good book is
Ian Smileys Making Pure Corn Whisky at
http://www.magma.ca/~smiley/main.htm, with full design details. See the list
of web resources below for links to sites selling ready-made stills. For
fuel alcohol stills see the Mother Earth Alcohol Fuel manual at
http://journeytoforever.org/biofuel_library/ethanol_motherearth/meToC.html,
and the The Manual for the Home and Farm Production of Alcohol Fuel by S.W.
Mathewson at

[biofuel] Still sizing

2001-06-14 Thread Ackland, Tony (CALNZAS)

Martin  Gaw  Peter ...

Some more comments on how to design a larger still.  Its a process where you
need to ask the right questions as you go through it.  The answers then
change how you proceed from there, or send you back to the start ...

1) What purity and flowrate do you want to produce at ?

So, for example, wanting 5 gal/day (19 L/day), do you want this in 12 hours
or 4 hours ?  Say you chose that you want it in 4 hours.  This means that
you want to collect your distillate at around 80 mL/min.

But you'll need a certain amount of reflux action happening, to get the
purity you require.  So we'll need a heat source which can actually generate
quite a bit more vapour than that.   But how much reflux ?  That going to
depend on the column design.

Normally I'd suggest that you'd use stainless steel wool/scrubbers for the
packing of the column.  These will give you about 1 HETP (theoretical stage
= equivalent to a single pot distillation) for each 13-15cm of packing.
Fine for small stills.  But, if you're into these high flowrates, and likely
to be using it quite frequently, if not daily, then may want something less
likely to block up/foul and is easier to clean.  Its also harder to pack a
wider column such that it will get a nice even flow over all the packing -
structured packing will do this easier for you if you're into large
diameters.  So then you're talking about using small marbles or rachig rings
or very short lengths of copper tubing (=homemade rachig tubes).  These have
greater HETP's and you may need 20-40cm of each to get the same purification
happening.

2) Depending on cleaning needs, etc decide on the type of packing

This will now make the column quite a bit taller (and a touch wider), if you
decided to use something less than stainless steel scrubbers.  

But there's a trick here.. extra height isn't really going to cost too much
more in the long run.  So why not go silly and make it quite a bit taller.
Say you've worked out, from
http://www.geocities.com/kiwi_distiller/refluxdesign.htm that you need to do
the equivalent of 8 stages/HETP's to get the purity you want.  These HETP's
are assuming a particular reflux ratio.  If you make the column taller
(guess, lets say 10-15 stages), then you can afford to run less reflux (and
downgrade how good the HETP's are), as you have surplice capacity to get the
purity you want.  E.g. so rather than needing to run at a reflux ratio of
say 4 (return 40 mL for every 10 mL you keep), you may be able to deliver
the same purity with a taller column running at a reflux ratio of 2.  This
will speed up your collection rate heaps.  It just means that you'll need a
wee ladder to read the top thermometer (why not use a thermocouple instead
?), and that your condenser will be up in the roof too ... (fun if you have
low water pressure)

Then you can use the calculator in
http://www.geocities.com/kiwi_distiller/dtw.htm#use_fract backwards ... e.g.
use it to estimate the heater size you need.  E.g. if you want 80 mL/min at
a reflux ratio of 4, then you'll need approx. 6.1 kW heat, but only 3 kW if
you only need a reflux ratio of 2.  So, even though its cost a little more
for the taller column, you'll save when trying to heat it.  A smaller
element also means that the column can be skinnier (thus not quite so much
packing etc required)  See how it sorta goes in circles ?

3) So you've picked your element size,

This then lets you estimate the column diameter from
http://www.geocities.com/kiwi_distiller/reflux_calc.htm
(remember just to beef it up slightly from that predicted).
Note that this calculator also estimates how long the pot will take to heat
up.  Consider using a second boost element in there if this time is too
long for you.

4) Size your condenser.

Once you know how much heat you're putting into the system, you then know
(exactly !) how much heat you have to take out of it (clue - its the same
amount).  Size your condenser to handle this .. see
http://www.geocities.com/kiwi_distiller/cond_calc.htm 

5) Pick the pot.

This won't really affect any of the above.  Just make sure you can
fill/empty/clean it ok.



In a nutshell, what I'm suggesting, is that if you want to make something
bigger than a usual hobby still, possibly down-grade the type of packing
you're going to use, but definitely make it heaps taller than what you would
usually.  This will allow you to run at a lower reflux ratio, and hence get
the through-put you're after, without needing a huge heat input.

Tony

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[biofuel] Still plans

2001-06-12 Thread Ackland, Tony (CALNZAS)

Martin,

For still plans I could suggest that you modify a Nixon-Stone still.
http://www.gin-vodka.com

See the photos section (page 1) at my site,
http://www.geocities.com/kiwi_distiller  for a couple of examples/versions
of it.

To get the purity, you will require a tall, well-packed column, and a good
control over the reflux ratio.  This still will do both those things.

I presently run one for drinking alcohol (its legal here in New Zealand).
However, it is not up to the quantity that you require.  With a 1380W heater
in it, I presently take about 93% alcohol at 40 mL/min (0.6 gal/hour).
Higher purity is easily achieved, but at a slower rate. Sounds like you'd be
more in the 2x or 3x version of this (3-4 kW) ?  To modify it would be only
a change in the column diameter (say to 2-2.5 inch ?) and a beefed up
condenser.

It would be a batch still operation, or are you after something more
continuous ?

Tony

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[biofuel] RE: Continuous still ?

2001-02-20 Thread Ackland, Tony (CALNZAS)

Sorry guys - forgot about diagrams getting removed in this NG

I've put my two concept sketches at
http://www.geocities.com/kiwi_distiller/image/cont.gif  (5 kB)
http://www.geoc4ities.com/kiwi_distiller/image/cont2.gif  (4 kB)

Tony

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RE: [biofuel] Corrosiveness of Alcohos?

2000-10-30 Thread Ackland, Tony (CALNZAS)


Does anyone have any other information on what corrosive 
effects alcohols have on engines or fuel pumps?  

Coulson, Richardson  Sinnott report that:

aluminium, aluminium bronze, brass, copper, gunmetal and bronze, high Si
iron, nickel, nickle-copper alloys, platinum, silver, stainless steel (18/8,
molybedenum,  austenitic ferric), titanium, tantalum, and zirconium, nylon
66 fibre  plastics, PCTFE, PTFE, polypropylene, and furane resin, hard
rubber, neophrene, nitrile rubber, chlorosulphinated polyethylene, and
silicone rubbers, concrete, glass, graphite, porcelain and stoneware, and
vitreous enamel 

are corrosion resistant to alcohols, beer  water up to 100C.

lead, mild steel (BSS 15), cast iron, and tin, acrylic sheet (eg perspex),
acrylonitrile butadiene styrene resins, rigid unplasticised PVC, plasticised
PVC, polyethylene (low  high density), polystyrene, melamine resins, epoxy
resin, phenol formaldehyde resins, polyester resins, butyl rubber 
halo-butyl rubber, ethylene propylene rubber, soft natural rubber, and
polyethylene rubber and wood
 
are not corrosion resistant to them. 

Tony
http://www.geocities.com/kiwi_distiller

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RE: [biofuel] marbles, Raschig rings, pot-scrubbers

2000-10-25 Thread Ackland, Tony (CALNZAS)

I agree here re scrubbers lacking thermal mass (heat capacity).  Once option
here, to maintain the delicate strata of temperatures in the column is to
make sure that the outside of the column is well insulated.  This way stray
wind gusts won't suddenly cause it to cool down unexpectedly  upset the
thermal profile.   

Some poor still designs rely on this side cooling of the column, so as to
cool some of the vapour and thus increase the reflux ratio a bit.
Unfortunately they're disrupting their efficiency in doing so.  Far better
to be doing any cooling and condensing above the packing, so that the column
has a nice even temperature gradient from the top (78 C ?) to its base (84 C
?) to allow a smooth transfer of ethanol to the vapour and water to the
liquid without having to overcome local heat losses.

See http://www.geocities.com/kiwi_distiller/heatmass.htm for a heat  mass
balance model/calculator for a typical 4 plate column (equivalent say to 1m
of marbles).  Dial up a bit of extra heat loss adjacent to one of the sides,
say half way up the column, and see how the vapour flowrate  purity will
decrease.

Tony

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RE: [biofuel] Lactose

2000-10-19 Thread Ackland, Tony (CALNZAS)

Can lactose (milk sugar) be fermented to make ethanol? 

I understand that most of the commercially made alcohol in New Zealand is
made from lactose. See : http://distillers.co.nz/html/pr34.html

I think however that it needs a particular yeast or enzyme to be able to do
it.

Tony

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RE: [biofuel] Small pilot plant details using A3 molecular sieve to create anhydrous ethanol

2000-07-20 Thread Ackland, Tony (CALNZAS)

David  Greg,
 
  While I know the basic theory  ... 
 
Could you please explain how they work ?  
How are they different to using adsorption (e.g. via lime or corn-grits etc)
 
Tony


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RE: [biofuel] Re: Biofuel list

2000-05-25 Thread Ackland, Tony (CALNZAS)

I had the same problem yesterday too - its simply the merger of Egroups and
Onelist. I had origianlly signed in via Onelist - now its Egroups wanting
the info.  Its explained on the sign-in page.  They (E/One) still know your
settings etc for your Groups, preferences etc.  Easily fixed just by signing
in, under the Egroups setup.

Tony


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