Re: [biofuels-biz] reducing ffa's

2003-08-12 Thread Michael Allen
Hi Ken, Calcium oxide also reacts with ffa and glycerides to make calcium soaps. These soaps are the basis of most greases used to lubricate moving machinery. Whereas sodium salts have the ability to disperse small amounts of oil into water, calcium (magnesium, zinc etc.) soaps have the abilit

Re: [biofuels-biz] reducing ffa's

2003-08-11 Thread Ken Gotberg
Hi Michael et al I’m wondering if anyone has looked at calcium oxide as a reactant/catalysis. CaO is very hydroscopic and should(?) suck up all the H2O and ffa’s. I’m thinking about this in order to use hydrated rice straw derived ethanol directly from fermentation rather than going through lab

Re: [biofuels-biz] reducing ffa's

2003-08-11 Thread Michael Allen
Dear Colton (and indirectly Girl Mark), I think pH meters are very stable and reliable instruments these days. But you have to rememebr that they measure the hydrogen ion concentration in a solvent that allows ionisation such as water. (Indeed, the pH scale is devised so that pH 7 is as neutra

RE: [biofuels-biz] reducing ffa's

2003-08-07 Thread pcampbell . tge
We are using a pH meter (& visual) methods during our titration to determine the ffa%. It is very frustrating since the pH meter readings are very inconsistant. Our current ffa% is 1.6% and we are trying to reduce it to .5% by acidification. Any comments on methods for determing the ffa%? Tha

RE: [biofuels-biz] reducing ffa's

2003-08-06 Thread Christopher Tan
How were you able to know that your ffa's increase? If you are just using a pH meter, it is but natural that the pH will fall since you are using a strong acid H2SO4. If you are titrating with NaOH, H2SO4 will eat up a considerable amount of lye. Christopher =>-Original Message- =>From:

Re: [biofuels-biz] reducing ffa's

2003-08-05 Thread Keith Addison
>hi all, > >I am trying to convert my free fatty acids to >esters by acidification using methanol and >H2SO4. Unfortunately, each time I try it, my >ffa level increases. >Is there anyone out there with a good >acidification recipe? http://journeytoforever.org/biodiesel_aleksnew.html Aleks Kac's