James,

There is a point, to which I am as yet certain, where higher than
atmospheric pressure must be implemented in order to get high ffa
feedstock to entirely convert in an esterification.

This would probably mean at least 4 atmospheres or greater. But
that doesn't amount to much as far as psi goes - 50+ pounds.

Todd

----- Original Message -----
From: James Slayden <[EMAIL PROTECTED]>
To: <biofuel@yahoogroups.com>
Sent: Tuesday, January 21, 2003 12:39 PM
Subject: Re: [biofuel] Where do I put all this glycerin??


> has anyone done any experimentation on reprocessing the FFA's
via the
> acid/base to see if it's convertable?  Although, I do like the
idea of
> burning it in a boiler/heater, it seems like it would be worthy
to capture
> it and make some more BD.
>
> James Slayden
>
> On Tue, 21 Jan 2003, Appal Energy wrote:
>
> > Probably about 6.715 gallons of true glycerin for every 85
> > gallons of feedstock. The rest will be recoverable alcohol
and
> > soap. Unfortunately you can't separate the glycerin from the
soap
> > without evaporating the glycerin at over 500*F. Journey to
> > Forever has a section on how to chemically recover the
glycerin,
> > a process that also breaks the soap down to the original free
> > fatty acids and changes the residual catalyst to a reusable
> > fertilizer.
> >
> > That same recovery process will require considerably less
> > chemical inputs and yield a slightly higher grade glycerin if
you
> > are originally using the acid/base process. Using the
straight
> > base process makes considerably more soap byproducts than the
> > acid/base process.
> >
> > Depending upon your feedstock, whether it was clean oil or
waste
> > fats and oils, the glycerin may be scent free enough as to
use in
> > other soap making or sell to soap makers, although they don't
use
> > a great deal of it. You may also be able to store it until
you
> > have enough volume for a glycerin refiner to take it. Or you
> > could dillute it with water and dispense it over fields along
> > with the recovered fertilizer.
> >
> > The recovered free fatty acids can be used as a boiler, oil
lamp
> > or some other fuel.
> >
> > Todd Swearingen
> >
> >
> > ----- Original Message -----
> > From: <[EMAIL PROTECTED]>
> > To: <biofuel@yahoogroups.com>
> > Sent: Monday, January 20, 2003 11:11 PM
> > Subject: [biofuel] Where do I put all this glycerin??
> >
> >
> > > Hello,
> > >
> > > I am very interested in making biodiesel from used
vegetable
> > oil and
> > > methanol, but my biggest concern is disposal of the
glycerin.
> > I
> > > understand I should obtain approximately 15 gallons of
> > glycering to
> > > every 85 gallons of biodiesel.  Is this correct?  And what
do I
> > do
> > > with all this glycerin?  Please help.
> > >
> > > Dave
> > >
> > >
> > >
> > > Biofuel at Journey to Forever:
> > > http://journeytoforever.org/biofuel.html
> > >
> > > Biofuels list archives:
> > > http://archive.nnytech.net/
> > >
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