Dear Keith and All

Unlike some other e-mails I'll descibe exactly
what I have done.

500cc virgin vegetable oil (non-specific type)
Heated to 35'C
80cc 99.5% Methanol added
Stirred for 5 minutes
Add 0.5cc (10 drops) of 97% H2SO4
Stir at 35'C for 1 hour - 600 rpm
Stir without heat for 1 hr - 600 rpm
Settle for 8 hrs
[ At all time the vessel has been covered with
tightly fitting cling film with only a very small
hole for the thermo-couple to go in (maybe 1.5 to
2mm diameter). Methanol loss is negligable. ]

No glycerine at all. The product has not settled
but is still liquid. This is virgin oil never
used fresh from the super market ASDA here, now
owned by WoolMart.

This morning - heated the oil to 55'C. Will add
3.1g NaOH plus 120cc of Methanol. If this turns
to jelly then I will repeat again and see what
happens.

The single stage process works a treat every
time, producing good clean ME. 

Keith, so the extra NaOH on top of that required
to drive the reaction neutralises the FFA's (in
used oil) and extracts them as soap in the final
wash?

Regards

Mark :-(


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