Sorry I should have added, that the issue occurs following refinement in 
refmac. (error in log file and SO4's are distorted)

_________________________________
Joel Tyndall, PhD

Senior Lecturer in Medicinal Chemistry
National School of Pharmacy
University of Otago
PO Box 56 Dunedin 9054
New Zealand
Skype: jtyndall

Ph: +64 3 479 7293

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