On Tue, 18 Mar 2025 09:21:44 +0100
Christian Buratto <[email protected]> wrote:

> Dear CCP4 community,
> I am currently trying to determine the structure of a
> protein-polyoxometalate complex. I am using a polyoxometalate
> molecule that is a derivative of the one deposited in the CCDC (ICSD:
> 173439). I am facing difficulties in generating a restraint file for
> this metal-oxo molecule that can be recognized by Phenix, both for
> ReadySet and refinement jobs. I have attempted to use ACEdrg and
> ELBOW, but all my trials have been unsuccessful. A common error in
> refinement states that Phenix is unable to determine the energy type
> for Ru or W atoms present in my ligand molecule. If anyone has any
> suggestions or alternative approaches, I would greatly appreciate
> your input! Thank you all for your time and help.
> Best regards,
> Christian
> 
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Dear Christian,

sounds like a perfect task for the grade server,
https://grade.globalphasing.org
in combination of babel. Usually, I generate a PDB file (e.g. with
PLATON or SHELXL), then use babel to convert to mol2
obabel -o mol2 -O yourligand.mol2 yourligand.pdb

and upload the mol2-file to the grade server. This honours your atom
naming. Make sure the PDB input file includes a residue name (which is
easily done with SHELXL). 
Cheers,
Tim

-- 
--
Tim Gruene
Head of the Core Facility Crystal Structure Analysis
Faculty of Chemistry
University of Vienna

Phone: +43-1-4277-70202

https://ccsa.univie.ac.at

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