Hi Peter

My thesis dates from 1996 and I'm no longer at that university. Scanning 250 
would be a major task. 

Also, while I want to see the difference between chemistry research language at 
that time and  current social informatics research language, I have a notion to 
lay out my thesis attractively, using InDesign. For that, I'd need the content 
in electronic format. Correcting OCRed files would be a major pain - there is 
page after page of stuff like the below

cheers

Bruce

d     Preparation of ylides

i      Preparation of [(ethanesulphinyl)ethoxycarbonylmethylene]triphenyl 
phosphorane 248

(Ethoxycarbonylmethylene)triphenylphosphorane 245 (12.4 g, 35 mmol) was stirred 
in dry toluene (100 ml) at 0°C under nitrogen.  Ethanesulphinyl chloride (1.9 
g, 17 mmol) in dry toluene (10 ml) was added and the mixture was stirred for 12 
h. The mixture was filtered and evaporation and trituration with ethyl acetate 
(5 ml) gave yellow cubes of slightly impure 
[(ethanesulphinyl)ethoxycarbonylmethylene]triphenylphosphorane 248 (1.2 g, 
16%).  m.p. 141–2°C (Found: C, 69.4; H, 5.9; m/z = 408.1307.  C24H25O3PS 
requires C, 67.9; H, 5.9%; M+ – O, 408.1313); dP +27.5 (120) [impurities +22.1 
(7) and 18.7 (3)]; dH (80 MHz) 7.4–8.0 (15H, m), 4.05 (2H, q, J = 7 Hz, OCH2), 
2.25 (2H, q of d, J = 7 Hz, JP = 2 Hz, SCH2), 0.95 (3H, t, J = 7 Hz, OCH2CH3) 
and 0.9–1.0 (3H, br s, SCH2CH3) [minor impurities 4.0–4.4 (m) and 1.2–1.4 (m)]; 
dC (75 MHz) 172.2 (C=O), 133.8 (6C, d, 2JP = 10 Hz), 131.7 (3C, d, 4JP = 2 Hz), 
130.8 (3C, 4ry, 1JP = 58 Hz), 128.3 (6C, d, 3JP = 12 Hz), 58.6 (OCH2), 37.0 (d, 
J = 120 Hz), 33.1 (SCH2), 13.9 (OCH2CH3) and 13.4; nmax 3040, 2970, 2920, 1640, 
1595, 1482, 1436, 1365, 1230, 1190, 1170, 1100, 1070 and 865 cm–1; m/z 408 (M+ 
– O, 45%), 379 (100), 301 (7), 277 (8), 262 (37), 183 (38), 152 (5), 108 (14) 
and 77(4).



On 27 Oct 2013, at 15:58, peter <pe...@petermwarner.com> wrote:

> Glad you got it sorted, but couldn't your university's library just scanned 
> it and e-mailed it to you???
> 
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