Dear James,
I agree with your chronology of the first full new protein structures by SR
MAD.
The 1975 two wavelength Hoppe and Jakubowksi study of erythrocruorin with Ni
and Co Kalpha Xray tubes is a classic piece of work of in effect MAD phasing .
See the IUCr Anomalous Scattering Conference
The first report of shooting a protein crystal at a synchrotron (I
think) was in 1976:
http://www.pnas.org/content/73/1/128.full.pdf
that was rubredoxin
The first PDB file that contains a SYNCHROTRON=Y entry is 1tld
(trypsin), which was deposited in 1989:
Thank you James, you should write a History book about the modern x-ray times.
Or better make one of those movies you are famous for.
Jürgen
On Mar 16, 2013, at 10:46 AM, James Holton wrote:
The first report of shooting a protein crystal at a synchrotron (I
think) was in 1976:
On Saturday, 16 March 2013, James Holton wrote:
The first report of shooting a protein crystal at a synchrotron (I
think) was in 1976:
http://www.pnas.org/content/73/1/128.full.pdf
that was rubredoxin
The first PDB file that contains a SYNCHROTRON=Y entry is 1tld
(trypsin), which was
Hi all - i'm sure this many will know this : when and what was the first
protein structure solved on a synchrotron?
Thanks in advance
Alan
--
Alan Cheung
Gene Center
Ludwig-Maximilians-University
Feodor-Lynen-Str. 25
81377 Munich
Germany
Phone: +49-89-2180-76845
Fax: +49-89-2180-76999
Hi
Not sure if this is strictly speaking the first protein *solved* on a
synchrotron, but I think this is the first report of shooting protein crystals
at a synchrotron in the widely available literature -
http://www.pnas.org/content/73/1/128.full.pdf+html
Phillips J C,
Did anyone see this prescient line in the PNAS paper? Seems that the MAD
concept was suggested way back then...
JPK
While the enhancement of anomalous scattering
has not yet been examined in detail, it is in principle
possible to use data collected at three wavelengths (15) to
completely solve
Nothing prescient about that. The MAD concept was first proposed by
Herzberg and Lau in 1967, much before sycnhrotrons were used for protein
crystallography.
Herzenberg, A. Lau, H. S. M. (1967) Acta. Crystallogr. 22, 24-28.
http://scripts.iucr.org/cgi-bin/paper?S0365110X6740
The PNAS
[mailto:CCP4BB@JISCMAIL.AC.UK] On Behalf Of Harry
Powell
Sent: 13 March 2013 15:04
To: ccp4bb
Subject: Re: [ccp4bb] first use of synchrotron radiation in PX
Hi
Not sure if this is strictly speaking the first protein *solved* on a
synchrotron, but I think this is the first report of shooting
:04
To: ccp4bb
Subject: Re: [ccp4bb] first use of synchrotron radiation in PX
Hi
Not sure if this is strictly speaking the first protein *solved* on a
synchrotron, but I think this is the first report of shooting protein
crystals at a synchrotron in the widely available literature
Dear Colleagues,
The paper
http://dx.doi.org/10.1107/S0108768185002233
in work led by Howard Einspahr undertaken at SRS 7.2 is a protein structural
specific result from synchrotron radiation.
The MAD method of course yielded totally specific to SR protein crystal
structures. The
To: ccp4bb
Subject: Re: [ccp4bb] first use of synchrotron radiation in PX
Hi
Not sure if this is strictly speaking the first protein *solved* on a
synchrotron, but I think this is the first report of shooting protein
crystals at a synchrotron in the widely available literature
Jean Witz (now deceased) once told me that the following paper is the first
one mentionning data collection on a synchrotron.
The journal is not really obscure and the paper should easily be found.
The work was done in Germany, if I remember well.
G. Rosenbaum, K.C. Holmes and J. Witz,
And indeed this experiment was done properly ... in a suit and tie!
http://www.embl-hamburg.de/aboutus/general_information/HH_about/history/HH-holmes.jpg
A.
PS The journal is indeed a bit obscure ...
On 13 Mar 2013, at 20:22, DUMAS Philippe (UDS) wrote:
Jean Witz (now deceased) once told
Nice account on the subject
J Synchrotron Radiat. 2010 July 1; 17(Pt 4): 433–444.
Published online 2010 May 14. doi: 10.1107/S0909049510011611
Impact of synchrotron radiation on macromolecular crystallography: a personal
view
Zbigniew Dauter,a,* Mariusz Jaskolski,b,* and Alexander Wlodawer,c,*
I never would have survived the dress code back then.
From: CCP4 bulletin board [CCP4BB@JISCMAIL.AC.UK] on behalf of Anastassis
Perrakis [a.perra...@nki.nl]
Sent: Wednesday, March 13, 2013 2:27 PM
To: CCP4BB@JISCMAIL.AC.UK
Subject: Re: [ccp4bb] first use
http://xdb.lbl.gov/Section2/Sec_2-2.html
Colin
-Original Message-
From: CCP4 bulletin board [mailto:CCP4BB@JISCMAIL.AC.UK] On Behalf Of DUMAS
Philippe (UDS)
Sent: 13 March 2013 19:22
To: ccp4bb
Subject: Re: [ccp4bb] first use of synchrotron radiation in PX
Jean Witz (now deceased) once
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