Re: FPSM : (was Re: [EXT] [External] Re: Step-like basline)

2023-09-07 Thread Luca Lutterotti
To be more clear, they did not ask for anything except that such a paper should never be published! Luca  Luca Lutterotti Dipartimento di Ingegneria Industriale Università di Trento via Sommarive, 9 - 38123 Trento (Italy) tel. +39 0461 2824-14 (Office), -34 (X-Ray lab)

Re: FPSM : (was Re: [EXT] [External] Re: Step-like basline)

2023-09-07 Thread Luca Lutterotti
No they did not, I think the reviewer was American, in fact he was also wining about unfair competition by the EU that provides funds to develop technologies directly competing against US companies….. The FPSM was originally developed in 2013-2014 inside one EU project. I would have not develope

RE: [EXT] Re: [External] Re: Step-like basline

2023-09-07 Thread Scott Speakman
Unrestricted Document Modeling of the absorption edge is also available in HighScore Plus v5.x However, as some have said, it is much better to avoid this artifact altogether. The energy discriminating linear detectors are good at filtering spectral contamination without introducing these arti

Re: FPSM : (was Re: [EXT] [External] Re: Step-like basline)

2023-09-07 Thread Reinhard Kleeberg
Dear Luca, the respect to your method was correctly referenced by Nicola in the Profex user manual, p. 8, since this method was (partially) implemented: https://www.profex-xrd.org/wp-content/uploads/2022/04/Profex-BGMN-Part-2-Application-EN.pdf In fact Joerg Bergmann and me have also tried simi

Re: Step-like basline

2023-09-07 Thread Matthew Rowles
Bad quality mono is always possible. I've got kb coming through with a current instrument. On Thu, 7 Sep 2023, 18:56 Reinhard Kleeberg, < kleeb...@mineral.tu-freiberg.de> wrote: > Hm, as Philips systems at this time always had combined a > scintillation counter with a diffracted beam graphite 002

Re: Step-like basline

2023-09-07 Thread Reinhard Kleeberg
Hm, as Philips systems at this time always had combined a scintillation counter with a diffracted beam graphite 002 bent monochromator, the question arises how the W L series and Cu Kbeta lines could reach the detector... Bad quality of the graphite mosaic crystal? Reinhard Zitat von Le

Re: Step-like basline

2023-09-07 Thread Le Bail Armel
The muscovite data is dated 1996 from an old Philips 1710 diffractometer,vertical sample holder, scintillation counter, not much used because wehad better instruments, hence this stupid test ;-)Armelenvoyé : 7 septembre 2023 à 10:57de : Reinhard Kleeberg à : rietveld_l@ill.frobjet : Re: Step-like

Re: Step-like basline

2023-09-07 Thread Reinhard Kleeberg
Dear Luca, sorry, I don't understand the "mosaic crystal" eplanation, especially not the "non-centre position" issue. IMHO, when the pattern was measured at a "powder" Bragg-Brentano configuration, in reflection mode, axial and equatorial divergence maximum ~ 2 degree, the 00l series of al

FPSM : (was Re: [EXT] [External] Re: Step-like basline)

2023-09-07 Thread Jonathan WRIGHT
Hi Luca, Thanks for sharing the links to your method - I hope we can try it the next time we get stuck on identification. It is a shame to hear you were delayed for so long by J.Appl.Cryst. Did they ask you to cite some work from the Glasgow group as the commercial competitor? I have in min