----- Original Message -----
From: Tom Parkhill <[email protected]>
To: <[email protected]>
Sent: Friday, 4 June 1999 03:08
Subject: RE: CS>yuck-o black stuff


> The black is caused (in my experience) from excessive current.
Also, 36
> volts is on the high side. Try putting a 10kOhm series resistor with
the 36
> volts. With a high impedance voltmeter across the electrodes, you
should see
> the voltage fall to 8-10 volts very soon.   My constant current
generator
> starts with an open circuit voltage of 30 volts, quickly falls to
8-10
> volts, and finishes at 3-4 volts.  At 10 MAmp, it takes only a few
hours to
> make a good batch. 2 mA takes 10-12 hours.  TomP
>
Tom

I agree, excessive current causes a dirty solution.
However, your currents and times do not correlate with mine. Of course
these factors depend upon electrode length, separation, water volume
etc.

My parameters are: electrodes 2mm, 45mm wetted depth, 45mm apart.
200mls d. water (7oz?).

30 volts, current limited to 0.75 mA
Hot water - 1 hr = 8 - 10 ppm

12 volts (9 V AC adaptor, not current limited)
Hot water - 1.5 hrs = 10 ppm rising to 15 after 24 hrs, final current
0.99 mA
Cold water - 3.0 hrs = 10 ppm, 10 ppm next day, final current 0.59 mA

Ivan


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