In a message dated 9/8/00 10:34:24 PM EST, [email protected] writes:

<< Subj:     Re: CS>HVAC CS
 Date:  9/8/00 10:34:24 PM EST
 From:  [email protected] (Robert L. Berger)
 Reply-to:  [email protected]
 To:    [email protected]
 
 Hi Roger;
 
 I machined down a #14 ga wire to 0.020 that is about 1/4" long and made a 
run with
 it.
 
 Today I have made four  2 liter HVAC arc with CO2 gas blanket all at 
diferent run
 times, as below.
 
 Minutes        Final conductance       Arc elect. dia.       T.E.            
  NO3
 (resolution 0.01 ppm from 0 to 20 ppm)
 
     60                36                            0.020"
 VVVW            0
 
     76                57                            0.063"
 VVVW            0
 
     90               55                            0.063"
 None              0
 
     110             47                            0.063"
 None              0
 
 The T.E. was measured in a total dark room (10:15 pm) in the basement with no
 lights. V= Very; W=Weak.
 
 In all cases the arc was blue. If any red or yellow shows up the NO3 will
 increase.

Bob: When I achieve sputtering the color is deep orange with sparks. I have 
analyzed for nitrate and nitrite several times and have found "below 
detection limit" or very close to it. Roger
 
 I have not had time to run Ag ppm but in the past it has followed rather 
closely
 to the final conductance.
 
 The finer arc point had no effect on the production rate.
 
 Are you using a  CO2 gas blanket or how are you generating the plasma? In 
what
 ambient?\

Bob: I do not use a protective blanket of any kind. Roger
 
 "Ole Bob" >>


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