--- anibal <[EMAIL PROTECTED]> wrote:
> heloo!!! again!!!
> i have another type of wvo.. this is liquid at room
> temperature.. it is
> black... very heavily used..
> i tried a mini batch of 500 ml..100 ml methanol..
> and from 5 to 10 grams of
> lye.. and it wont react... the more lye.. the more
> it seemed to want to
> react but.. nothing happened overnight,,,
> any thoughts? on what might be the problem?
> maybe the oil is stale? maybe it has too much
> water?>
> my methanol. is about 98% percent it has been going
> well in other
> reactions..
> should i add more lye?
> thanks for the info!!
> anibal
>
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Anibal
do you heat the oil to 54C before adding sodium
methoxide.
you only need 3.25g of NaOH for 500ml of wvo.
At 54C mix for 20 min.
fox
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