You would be well advised to do some background reading on microabsorption as it will be pretty bad with those two phases and limit the accuracy you may realistically expect in your quantification
Pam From: rietveld_l-requ...@ill.fr [mailto:rietveld_l-requ...@ill.fr] On Behalf Of Nelson Sent: Friday, September 05, 2014 12:44 PM To: rietveld_l@ill.fr Subject: Quantification and rietveld refinement Dear rietvelds I have some samples, all with the same two phases: alumina and crocoite (PbCrO4) (electrochemical bath). I use Cobalt radiation. Indexing, I use always the same two ICDD files, 74-0323 for alumina and 73-1332 for crocoite. I use software High score plus. Can i use the semiquantification of software for know the quantification of each phase betwen the samples. Wuhere i can find the right cif files for this two phases, for introduce in High score plus and made Rietveld refinement. Where i can find a manual or exemples of how to make a rietveld refinement of this XRD. I don´t have experience of rietveld analysis. Thanks in advances Best regrds Nelson
++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++ Please do NOT attach files to the whole list <alan.he...@neutronoptics.com> Send commands to <lists...@ill.fr> eg: HELP as the subject with no body text The Rietveld_L list archive is on http://www.mail-archive.com/rietveld_l@ill.fr/ ++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++
