Frank,
ref your "A rather misinformed comment, wouldn't you say, given the fact
that there is a size distribution plot that clearly shows a huge volume peak
at 2.4 nm that is available for all to see".....
why not send me a sample of that specially prepared sample and we'll make
available and/or publish micrographs of it ....for all to see!
Stephen

> -----Original Message-----
> From: Frank Key [mailto:fr...@strsoft.com]
> Sent: Friday, March 30, 2001 1:46 PM
> To: silver-list@eskimo.com
> Subject: Re: CS>Commercial Product Reports
>
>
> Stephen wrote:
>
>
> > > If there are 2 nm particles in the colloid, the Zetasizer has
> no problem
> > > finding them.
> >
> > The scales don't even start [on the products you chose] below
> 3.7nm -- and
> > there is "0" data smaller than 27nm shown!
>
> That is what is called "auto scaling", modern scientific
> instruments do that sort of thing. If there is no data, then
> nothing is reported.
>
> Please notice on the Smalltest sample, the auto scaling choose a
> minimum value to report of 1.3 nm.
>
> > My comments were directed to the reports you had previously published on
> > your website, not something just concocted to rebut an argument!
>
> Auto scaling works the same on all the runs, it is a standard
> feature that is always enabled.
>
>
> > Then, what do you suppose happened to the particles that were
> visible, if
> > only faintly, in the Tyndall prior to evaporation?
>
> Since the particles of silver oxide outnumber the "real
> particles" by several million to one, they simply make
> observation of the "real particles" very difficult, if not impossible.
>
> > The Zetasizer was designed for particle sizing in "bulk analysis", NOT
> > particle characterization -- as I was informed.
>
> Bulk analysis means the aggregate solution, which is precisely
> what is desired for particle size distribution. Size distribution
> is but one parameter of complete characterization of colloidal
> particles, and a very important parameter. Zeta potential is
> another very important parameter in characterizing colloids.
>
> > No, Frank, not evaluation; just raw data.  No Qualitative
> analysis whatever!
> > And no pH data....
>
> Sorry about that, the pH data will be forthcoming shortly, I
> wanted to get a new pH probe operational and doing so has not
> been the highest priority.
>
> The pH data does not change any of the data presented and makes
> no material change to the picture that can be drawn from the
> information presented thus far.
>
>
> > No, it doesn't demonstrate that that.... [As I said above] the
> scales don't
> > even start below 3.7 nm
>
> See the brief description of "auto scaling" above.
>
> > Again, not so, the Zetasizer does not "see" particles in the nanometer
> > range -- per Malvern Instruments.
>
> A rather misinformed comment, wouldn't you say, given the fact
> that there is a size distribution plot that clearly shows a huge
> volume peak at 2.4 nm that is available for all to see at:
>
> http://www.silver-colloids.com/Misc/Smalltest.html
>
> Given your exceptional eyesight (able to see micron particles
> with the naked eye), you too may be able to see the numbers on
> the plot and in the corresponding table of values on page 2 of
> the size report.
>
> Please notice the table lists 1.3 nm as the smallest reported value.
> Isn't auto scaling a wonderful thing!
>
>
> > Great, it's something to look forward to....
>
> I will take that as a positive comment, thank you!
>
>
> frank key
>
>
>
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